A new protocol is reported for the synthesis of a heterogeneous palladium nanocomposite sta
bilized with a terephthalic acid-derived lig
and (
N,
N-
bis(4-hydroxy-3-methoxy
benzylidene)terephthalohydrazide). This is a highly insolu
ble lig
and in common organic solvents, except dimethylformamide
and brary/content/render" xmlns:mml="http://www.w3.org/1998/Math/MathML" id="aoc3549-eo-2001">dimethylsulfoxide. The resulting palladium nanocomposite acts as an efficient catalyst precursor for Mizoroki–Heck
coupling reactions conducted under various reaction conditions. The spectral data suggest that the rate, yield
and recycling of the catalyst are more effective for
C–C coupling reactions. Copyright