Multi-mycotoxins analysis in Pheretima using ultra-high-performance liquid chromatography tandem mass spectrometry based on a modified QuEChERS method
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- 作者：Sisi Zhanga ; b ; 14211030033@fudan.edu.cn" class="auth_mail" title="E-mail the corresponding author ; Jiwei Lub ; lujiwei1011@163.com" class="auth_mail" title="E-mail the corresponding author ; Shaomin Wangb ; wangshaomin2008@163.com" class="auth_mail" title="E-mail the corresponding author ; Dan Maob ; m21944@126.com" class="auth_mail" title="E-mail the corresponding author ; Shui Miaob ; qmiao2008@163.com" class="auth_mail" title="E-mail the corresponding author ; Shen Jib ; jishen2016@126.com" class="auth_mail" title="E-mail the corresponding author (Chief Pharmacist ; PhD Supervisor)
- 关键词：QuEChERS ; quick easy cheap effective rugged and safe ; FB1 ; fumonisin B1 ; FB2 ; fumonisin B2 ; FB3 ; fumonisin B3 ; AFB1 ; aflatoxin B1 ; AFB2 ; aflatoxin B2 ; AFG1 ; aflatoxin G1 ; AFG2 ; aflatoxin G2 ; OTA ; ochratoxinA ; OTB ; ochratoxin B ; DOM-1 ; de-epoxy-deoxynivalenol ; α-ZOL ; α-zearalenol ; β-ZOL ; β-zearalenol ; ZAN ; zearalanone ; ZEA ; zearalenone ; 13C-ZEA ; 13C-zearalanone ; α-ZAL ; α-zearalanol ; β-ZAL ; β-zearalanol ; DON ; deoxynivalenol ; 3-ADON ; 3-acetyldeoxynivalenol ; 15-ADON 15-Acetyldeoxynivalenol ; Fus-X ; F
- 刊名：Journal of Chromatography B, Analytical Technologies in the Biomedical and Life Sciences
- 出版年：2016
- 出版时间：1 November 2016
- 年：2016
- 卷：1035
- 期：Complete
- 页码：31-41
- 全文大小：2902 K
文摘
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A sensitive and high-throughput method was established and validated for simultaneous determination of 22 mycotoxins under MRM mode.
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Pheretima samples were prepared by modified QuEChERS method with high recoveries for all target analytes.
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The lowest limits of detection varied from 0.05 μg kg−1 to10 μg kg−1.
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Q/q ratio was used for additional confirmation of FB1 and FB2 contamination at 2.54–3.78 μg/kg.
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This method could be extended to the analysis of mycotoxins in other complex matrices.