Cuprous chloride (CuCl) was prepared on Cu substrate by chemical bath deposition.
HCl dip treatments facilitated the deposition of a full-coverage CuCl film.
A homogeneous elemental distribution was recognized for the deposited CuCl layer.
Excitonic and biexcitonic photoluminescence lines of CuCl films were well-resolved.
The free exciton emission line of CuCl films was observable at room temperature.
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