Cloud-point extraction is compatible with liquid chromatography coupled to electrospray ionization mass spectrometry for the determination of antazoline in human plasma
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- 作者：Joanna Giebułtowicza ; joanna.giebultowicz@wum.edu.pl" class="auth_mail" title="E-mail the corresponding author ; Grzegorz Kojroa ; b ; Roman Piotrowskic ; Piotr Kułakowskic ; Piotr Wroczyńskia
- 关键词：AF ; atrial fibrillation ; AN-PAF ; single center ; randomized ; double blind ; placebo-controlled study of clinical efficacy of antazoline in rapid cardioversion of paroxysmal atrial fibrillation ; CPE ; cloud-point extraction ; CMC ; critical micelle concentration ; ESI ; electrospray ionization ; HPLC ; high-performance liquid chromatography ; IS ; internal standard ; LC&ndash ; MS ; liquid chromatography coupled to mass spectrometry ; LLE ; liquid-liquid extraction ; LOD ; limit of detection ; LLOQ ; lower limit of q
- 刊名：Journal of Pharmaceutical and Biomedical Analysis
- 出版年：2016
- 出版时间：5 September 2016
- 年：2016
- 卷：128
- 期：Complete
- 页码：294-301
- 全文大小：1110 K
文摘
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Simple, environmentally friendly sample preparation by cloud-point extraction (CPE).
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Evaluation of the direct influence of Triton on the ME for analytes.
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First use of the CPE to determine the concentration of antazoline in human plasma.
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Positive outcome of comparison of CPE with LLE.
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