Amine-free silylation of alcohols under 4-methylpyridine N-oxide-catalyzed conditions

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• 作者：Keisuke Yoshida ; ^{yoshida@applc.keio.ac.jp" class="auth_mail" title="E-mail the corresponding author} ; Yuta Fujino ; Yukihiro Itatsu ; Hiroki Inoue ; Yohei Kanoko ; Ken-ichi Takao ; ^{takao@applc.keio.ac.jp" class="auth_mail" title="E-mail the corresponding author}
• 关键词：Amine-free ; Silylation ; 4-Methylpyridine N-oxide ; MS4A
• 刊名：Tetrahedron Letters
• 出版年：2016
• 出版时间：3 February 2016
• 年：2016
• 卷：57
• 期：5
• 页码：627-631
• 全文大小：991 K

文摘

Amine-free silylation of various alcohols catalyzed by 4-methylpyridine N-oxide in the presence of MS4A at room temperature was developed. This simple method gave various silyl ethers in a high yield.