Direct coupling of a flow-flow electromembrane extraction probe to LC-MS
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- 作者：David Fuchsa ; Charlotte Gabel-Jensena ; Henrik Jensena ; Kasper D. Randa ; Stig Pedersen-Bjergaarda ; b ; Steen Honoré ; Hansena ; Nickolaj Jacob Petersena ; nickolaj.petersen@sund.ku.dk" class="auth_mail" title="E-mail the corresponding author
- 关键词：Electromembrane exraction (EME) ; EME-LC-MS ; Supported liquid membrane (SLM) ; On-line/in-line sample preparation ; In-vitro drug metabolism ; Methadone metabolism
- 刊名：Analytica Chimica Acta
- 出版年：2016
- 出版时间：28 January 2016
- 年：2016
- 卷：905
- 期：Complete
- 页码：93-99
- 全文大小：1305 K
文摘
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An in-line Electromembrane Extraction – LC-MS system was developed
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Hyphenation of the Electromembrane extraction probe and the LC-MS system was accomplished using a 10-port switching valve
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The system integrates a complete analytical workflow of rapid extraction, enrichment, separation and detection of analytes
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The setup was used to monitor the in-vitro metabolism of methadone by rat liver microsomes