QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS
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- 作者：Edouard Akono Nantiaa ; 1 ; David Moreno-Gonzá ; lezb ; 1 ; Faustin P.T. Manfoc ; Laura Gá ; miz-Graciab ; Ana M. Garcí ; a-Campañ ; ab ; amgarcia@ugr.es" class="auth_mail" title="E-mail the corresponding author
- 关键词：3-CF ; 3-hydroxy carbofuran ; MeCN ; acetonitrile ; ALD ; aldicarb ; ALDSFN ; aldicarb sulfoxide ; ASL ; asulam ; BFU ; benfuracarb ; BTH ; benthiocarb ; CRB ; carbamate ; CAR ; carbaryl ; CBZ-BY ; carbendazim-benomyl ; CY ; cymoxanil ; DETH ; diethofencarb ; dSPE ; dispersive solid phase extraction ; ESI ; electrospray ionization ; EtOAc ; ethylacetate ; ETH ; ethiofencarb ; FEN ; fenobucarb ; FNX ; fenoxycarb ; FURA ; furathiocarb ; GBC ; graphitized carbon black ; ISO ; isoprocarb ; LOQ ; limit of quantification ; ME ; matrix effect ; MR
- 刊名：Food Chemistry
- 出版年：2017
- 出版时间：1 February 2017
- 年：2017
- 卷：216
- 期：Complete
- 页码：334-341
- 全文大小：733 K
文摘
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Twenty-eight carbamates in aromatic herbs by UHPLC-MS/MS analysis.
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Development of QuEChERS as cheap and efficient method for extraction and clean up.
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Trueness of the method in parsley, basil, mint, thyme and salvia.
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LOQs below 3.4 μg kg−1 and recoveries between 60 and 125%.
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Occurrence study in different fresh aromatic herbs from Spain and Cameroon.
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