Reflux-based synthesis and electrocatalytic characteristics of nickel phosphate nanoparticles

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• 作者：Mohammed A. Al-Omair^a ; A.H. Touny^a ; ^c ; M.M. Saleh^a ; ^b ; ^{mmsaleh@kfu.edu.sa} ; ^{mahmoudsaleh90@yahoo.com}
• 关键词：Nickel phosphate ; Nanoparticles ; Urea ; Electrocatalytic ; Oxidation
• 刊名：Journal of Power Sources
• 出版年：2017
• 出版时间：28 February 2017
• 年：2017
• 卷：342
• 期：Complete
• 页码：1032-1039
• 全文大小：1204 K
• 卷排序：342

文摘

Nickel phosphate (NiPh) nanoparticles were synthesized using reflux-based method. XRD pattern and FTIR spectrum suggests Ni3(PO4)2.8H2O phase. It has monoclinic crystallographic form and it was casted on glassy carbon (GC). GC/NiPh demonstrates electrocatalytic activity toward urea oxidation in 0.5 M KOH.