Salting-out assisted liquid-liquid extraction coupled to ultra-high performance liquid chromatography-tandem mass spectrometry for the determination of tetracycline residues in infant foods
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- 作者：David Moreno-Gonzá ; lez ; Ana M. Garcí ; a-Campañ ; a ; amgarcia@ugr.es
- 关键词：ACO ; acetone ; ACN ; acetonitrile ; CTC ; chlortetracycline ; CAD ; collision gas ; CEP ; collision cell entrance potential ; CE ; collision energy ; CXP ; collision exit potential ; I ; confirmation ion ; CCα ; decision limit ; DP ; declustering potential ; CCβ ; detection capability ; DC ; doxycycline ; ESI ; electrospray ionization ; EP ; entrance potential ; EU ; European Union ; MS ; mass spectrometry ; ME ; matrix effect ; MRL ; maximum residue limit ; MIF ; meat-based infant food ; MTC ; methacycline ; MeOH ; methanol ; MRM ; mul
- 刊名：Food Chemistry
- 出版年：2017
- 出版时间：15 April 2017
- 年：2017
- 卷：221
- 期：Complete
- 页码：1763-1769
- 全文大小：406 K
- 卷排序：221
文摘
Tetracycline determination in infant products by UHPLC–MS/MS. Optimization of SALLE by experimental design. Validation of the method in infant products based on meat and vegetables or milk. LOQs between 0.16 and 0.48 μg kg−1 with RSD values lower than 7.3%.