A simple, accurate, time-saving and green method for the determination of 15 sulfonamides and metabolites in serum samples by ultra-high performance supercritical fluid chromatography
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- 作者：Yuan Zhanga ; b ; 13840149878@163.com" class="auth_mail" title="E-mail the corresponding author ; Wei-E Zhoua ; Shao-Hui Lia ; Zhi-Qin Rena ; Wei-Qing Lia ; Yu Zhoub ; Xue-Song Fengb ; Wen-Jie Wua ; Feng Zhanga ; fengzhang@126.com" class="auth_mail" title="E-mail the corresponding author ; fengzhangchem@yahoo.com" class="auth_mail" title="E-mail the corresponding author
- 关键词：Sulfonamides ; Ultra-high performance supercritical fluid chromatography (UHPSFC) ; PDA ; Serum ; Resolution
- 刊名：Journal of Chromatography A
- 出版年：2016
- 出版时间：5 February 2016
- 年：2016
- 卷：1432
- 期：Complete
- 页码：132-139
- 全文大小：1331 K
文摘
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Near baseline separation for 15 sulfonamides and metabolites by UHPSFC was achieved.
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Stationary phases, modifiers, additives, column temperature, ABPR backpressure and flow rate were optimized for baseline separate 15 sulfonamides.
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UHPSFC-PDA for determination 15 sulfonamides and metabolites in serum.
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Simple, accurate, green, low cost, faster separations and better resolution.
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Assumed that the retention behavior of sulfonamides on BEH column may mainly depend on the molecule polarity.
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