Production Scaleup of Reverse Micelle Synthesis
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- 作者：Shannon A. Morrison ; Christopher L. Cahill ; Everett E. Carpenter ; and Vincent G. Harris
- 刊名：Industrial & Engineering Chemistry Research
- 出版年：2006
- 出版时间：February 1, 2006
- 年：2006
- 卷：45
- 期：3
- 页码：1217 - 1220
- 全文大小：229K
- 年卷期：v.45,no.3(February 1, 2006)
- ISSN：1520-5045
文摘
A wide range of techniques for the successful synthesis of nanosized materials have been developed recently.These procedures are sufficient for normal scientific investigation; however, for these materials to beincorporated into any practical application, the process for making them must be scalable to a larger volume.In this work, we focus on a published recipe for manganese zinc ferrite (MZFO) nanoparticles, which usesthe reverse micelle synthesis technique. The normal bench-top synthesis has been scaled by a factor of 40and successfully adapted to a 30-L pilot plant. The product of this synthesis is similar to the bench-top sample,which is also comparable to a ceramic MZFO standard. Through this work, we have demonstrated that thereverse micelle process is scalable to larger volumes.