Functionalized Multiwalled Carbon Nanotube as Dispersive Solid-Phase Extraction Materials Combined with High-Performance Liquid Chromatography for Thiabendazole Analysis in Environmental and Food Samples

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• 作者：Xu Xu ; Na Long ; Junna Lv ; Lingling Wang ; Minhui Zhang ; Xinyu Qi…
• 关键词：Triabendazole ; Pesticides residues ; Dispersive solid ; phase extraction ; Functionalized multiwalled carbon nanotube ; Environmental and food samples
• 刊名：Food Analytical Methods
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：9
• 期：1
• 页码：30-37
• 全文大小：1,234 KB
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• 作者单位：Xu Xu (1)
  Na Long (1)
  Junna Lv (1)
  Lingling Wang (1)
  Minhui Zhang (1)
  Xinyu Qi (1)
  Lei Zhang (1)
  
  1. College of Chemistry, Liaoning University, 66 Chongshan Middle Road, Shenyang, 110036, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

A modified Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) method based on the dispersive solid-phase extraction (dSPE) combined with high-performance liquid chromatography (HPLC) was developed for the determination of thiabendazole (TBZ) in environmental and food samples. Hydroxyl functionalized multiwalled carbon nanotube (MWCNT-OH) was used as dSPE material for the preconcentration of analyte. Several experimental parameters, including the amount of sorbent, extraction time, the pH and ionic strength of sample solution, and desorption conditions, were evaluated. Under optimal experimental conditions, good linearity was observed in the range of 10–1000 ng mL−1 with the correlation coefficient of 0.9962. The limit of detection and quantification were 2.6 and 8.7 ng mL−1, respectively. The present method was applied to the analysis of different environmental and food samples, and the recoveries of TBZ obtained were in the range of 92.9–103.9 % with the relative standard deviations lower than 6.5 %. The results showed that the proposed method was a rapid, convenient, and feasible method for the determination of TBZ in environmental and food samples. Keywords Triabendazole Pesticides residues Dispersive solid-phase extraction Functionalized multiwalled carbon nanotube Environmental and food samples