Synthesis and characterization of glyceryl monooleate-based polyester

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• 作者：Puyou Jia ; Caiying Bo ; Lihong Hu ; Yonghong Zhou
• 关键词：Polyester ; Poly(vinyl chloride) ; Blends ; Thermal Stability
• 刊名：Korean Journal of Chemical Engineering
• 出版年：2015
• 出版时间：March 2015
• 年：2015
• 卷：32
• 期：3
• 页码：547-551
• 全文大小：301 KB
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• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Industrial Chemistry and Chemical Engineering
  Catalysis
  Materials Science
  Biotechnology
  
• 出版者：Springer New York
• ISSN：1975-7220

文摘

A unique biobased polyester poly(succinic acid-glyceryl monooleate) (PSAGMO) was synthesized and characterized from succinic acid (SA) and glyceryl monooleate (GMO). The polyester was characterized by gel permeation chromatography (GPC), Fourier transform infrared spectroscopy (FTIR) and nuclear magnetic response spectroscopy (NMR). The polyester was used as the plasticizer of poly (vinyl chloride) (PVC). The mechanical properties and the thermodynamic properties of the blends were characterized. The TG-DTA data indicated that the thermal degradation temperature (T d ) of PVC blends plasticized with PSAGMO could increase from 249.3 °C to 255.6 °C. The DMA showed that the glass transition temperature (Tg) of the PVC blends decreased from 49.5 °C to 35 °C. The mechanical properties indicated that the PSAGMO could decrease the tensile strength and increase the elongation at break of the PVC blends. This study may lead to the development of new type of PVC plasticizer based on renewable resource.