Ruthenium catalysts based on mesoporous aromatic frameworks for the hydrogenation of arenes

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• 作者：Anton Maximov ; Anna Zolotukhina…
• 关键词：Catalysis ; Ruthenium nanoparticles ; Porous aromatic frameworks ; Arenes ; Size ; selective hydrogenation
• 刊名：Reaction Kinetics, Mechanisms and Catalysis
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：117
• 期：2
• 页码：729-743
• 全文大小：1,456 KB
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• 作者单位：Anton Maximov (1)
  Anna Zolotukhina (1)
  Leonid Kulikov (1)
  Yulia Kardasheva (1)
  Eduard Karakhanov (1)
  
  1. Department of Petroleum Chemistry and Organic Catalysis, Moscow State University, Leninskiye Gory 1-3, GSP-1, Moscow, Russian Federation, 119991
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Industrial Chemistry and Chemical Engineering
  Physical Chemistry
  
• 出版者：Akad茅miai Kiad贸, co-published with Springer Science+Business Media B.V., Formerly Kluwer Academic
• ISSN：1878-5204

文摘

Novel catalysts consisting of ruthenium nanoparticles supported on diamond-like porous aromatic frameworks (PAFs) with 3 and 4 benzene rings in the edges have been synthetized with a narrow particle size distribution (0.85 and 1.10 nm respectively). Several techniques, such as N₂ physisorption, Fourier transform infrared spectroscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, and solid-state nuclear magnetic resonance were used for characterizing the synthesized materials. The obtained catalysts appeared to be active in the hydrogenation of various aromatic substances (specific catalytic activity reached activities up to 2660 mol_(Sub) h−1 mol _(Ru) −1 in the case of phenol). Notably, a size-selective hydrogenation was observed for catalysts based on PAFs.