Studies on Preparation and Hydrogen Storage Properties of Dual-Metal Ferrocenyl Coordination Polymer Microspheres

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• 作者：Ruoli Sun ; Li Wang ; Haojie Yu ; Zain-ul-Abdin…
• 关键词：Hydrogen storage ; Microspheres ; Ferrocenyl coordination polymers
• 刊名：Journal of Inorganic and Organometallic Polymers and Materials
• 出版年：2016
• 出版时间：May 2016
• 年：2016
• 卷：26
• 期：3
• 页码：545-554
• 全文大小：2,315 KB
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• 作者单位：Ruoli Sun (1)
  Li Wang (1)
  Haojie Yu (1)
  Zain-ul-Abdin (1)
  Yongsheng Chen (1)
  Hamad Khalid (1)
  Nasir M. Abbasi (1)
  Muhammad Akram (1)
  Sergey Z. Vatsadze (2)
  Dmitri A. Lemenovskii (2)
  
  1. State Key Laboratory of Chemical Engineering, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou, 310027, People’s Republic of China
  2. Department of Chemistry, M.V. Lomonosov Moscow State University, Leninskie Gory, 1-3, Moscow, Russian Federation, 119992
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Inorganic Chemistry
  Organic Chemistry
  Polymer Sciences
  
• 出版者：Springer New York
• ISSN：1574-1451

文摘

A series of dual-metal ferrocenyl coordination polymer microspheres (M<sub>1sub>M<sub>2sub>-CPMs, M<sub>1sub>M<sub>2sub> = CoMn, CoCu, MnCu) were synthesized by the reaction of 1,1′-ferrocene dicarboxylic acid with mixed metal salts via solvothermal method. From SEM and TEM images, it was found that all the as-synthesized coordination polymers showed microspheres structures. The products were also characterized by X-ray photoelectron spectroscopy (XPS), fourier transform infrared (FT-IR), powder X-ray diffraction (PXRD) and thermogravimetric analysis (TGA). The M<sub>1sub>M<sub>2sub>-CPMs showed good thermostability and remained stable up to 250 °C. These M<sub>1sub>M<sub>2sub>-CPMs exhibited hydrogen uptake capacity. More interestingly, through the comparison among three microspheres we found that the M<sub>1sub>M<sub>2sub>-CPMs with hollow structures showed better hydrogen uptake.