Determination of indometacin and acemetacin in human urine via reduced graphene oxide - based pipette tip solid-phase extraction coupled to HPLC
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- 作者：Yanan Yuan ; Ning Sun ; Hongyuan Yan ; Dandan Han ; Kyung Ho Row
- 关键词：Anti ; inflammatory drug ; Urine analysis ; Multi ; walled carbon nanotubes ; HLB sorbent ; Strong cation exchange chromatography ; SCX ; Nanomaterial
- 刊名：Microchimica Acta
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：183
- 期：2
- 页码：799-804
- 全文大小：723 KB
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Ning Sun (1) (2)
Hongyuan Yan (1) (2)
Dandan Han (1)
Kyung Ho Row (3)
1. Department of Preventive Medicine and Health Management, Key Laboratory of Medicinal Chemistry and Molecular Diagnosis, Hebei University, Baoding, 071002, China
2. Key Laboratory of Pharmaceutical Quality Control of Hebei Province, College of Pharmacy, Hebei University, Baoding, 071002, China
3. Department of Chemistry and Chemical Engineering, Inha University, Incheon, 402751, South Korea - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Analytical Chemistry
Inorganic Chemistry
Physical Chemistry
Characterization and Evaluation Materials
Monitoring, Environmental Analysis and Environmental Ecotoxicology - 出版者：Springer Wien
- ISSN：1436-5073
文摘
A rapid method for solid-phase extraction (SPE) and quantitation of the non-steroidal anti-inflammatory drugs indometacin and acemetacin in urine was developed. SPE is based in of the use of a reduced graphene oxide (rGO) in a pipette tip, and separation and quantitation is based on HPLC with a Promosil C18 column and UV detection. The amount of sorbent, types and volumes of washing solvent and elution solvent were optimized. The results showed that the use of the rGO sorbent and a miniaturized pipette tip cartridge are distinctly superior to other sorbents including multiwalled carbon nanotubes and conventional SPE cartridges. Linear responses to indometacin and acemetacin are found for the 0.1–50 μg mL−1 concentration ranges, recoveries (at three spiking levels) range from 89.6 % to 95.7 %, and the relative standard deviations are ≤6.4 %.