One-pot, three-component, green procedure for efficient synthesis of allomaltol derivatives

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• 作者：Yu-Ling Li ; Kai Wang ; Bo Zhao ; Qiu-Shi Jiang…
• 关键词：MCRs ; Allomaltol derivatives ; Synthesis ; Ionic liquid
• 刊名：Research on Chemical Intermediates
• 出版年：2015
• 出版时间：August 2015
• 年：2015
• 卷：41
• 期：8
• 页码：5149-5158
• 全文大小：416 KB
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• 作者单位：Yu-Ling Li (1)
  Kai Wang (1)
  Bo Zhao (1)
  Qiu-Shi Jiang (1)
  Bai-Xiang Du (1)
  Cai-Fa Chen (1)
  
  1. The Key Laboratory of Biotechnology for Medicinal Plants of Jiangsu Province, School of Chemistry and Chemical Engineering, Jiangsu Normal University, Xuzhou, 221116, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Physical Chemistry
  Inorganic Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1568-5675

文摘

We report an efficient, mild, one-pot, three-component method, catalyzed by Et3N in the ionic liquid [bmim+][BF4 ?/sup>], for synthesis of 2-[(aryl)-(3-hydroxy-6-methyl-4-oxo-4H-pyran-2-yl)methyl]indan-1,3-diones from aromatic aldehydes, 1,3-indanedione, and 5-hydroxy-2-methyl-4H-pyran-4-one. The method has the advantages of high yields, mild reaction conditions, convenient operation, and environmental friendliness.