Preparation and characterization of hybrid polycaprolactone/cellulose ultrafine fibers via electrospinning
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- 作者：Shamshad Ali (1) (2)
Zeeshan Khatri (2) (3)
Kyung Wha Oh (4)
Ick-Soo Kim (3)
Seong Hun Kim (1) - 关键词：poly(? ; caprolactone) ; cellulose acetate ; cellulose ; electrospinning ; wettability ; ultrafine fibers
- 刊名：Macromolecular Research
- 出版年：2014
- 出版时间：May 2014
- 年：2014
- 卷：22
- 期：5
- 页码：562-568
- 全文大小：
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Zeeshan Khatri (2) (3)
Kyung Wha Oh (4)
Ick-Soo Kim (3)
Seong Hun Kim (1)
1. Department of Organic and Nano Engineering, Hanyang University, Seoul, 133-791, Korea
2. Department of Textile Engineering, Mehran University of Engineering and Technology, Jamshoro, 76062, Pakistan
3. Nano Fusion Technology Research Group, Faculty of Textile Science and Technology, Shinshu University, 3-15-1, Tokida, Ueda, Nagano, 386-8567, Japan
4. Department of Fashion Design, Chung-Ang University, Gyeonggi, 456-756, Korea - ISSN：2092-7673
文摘
A series of poly(?-caprolactone) (PCL)/cellulose acetate (CA) ultrafine fiber webs were prepared via electrospinning followed by deacetylation in an aqueous alkaline solution to convert CA into cellulose (CEL). The wetting properties of PCL/CA and PCL/CEL blends were evaluated to investigate wicking behavior. The results showed that the conversion of PCL/CA into PCL/CEL leads to an improved wettability. Attenuated total reflectance-Fourier transform infrared (ATR-FTIR) study revealed that CA was completely converted into CEL after deacetylation, and PCL/CEL blends exhibited characteristics peaks of both constituent fibers. The differential scanning calorimetry (DSC) analysis demonstrated that the PCL/CA ultrafine fibers were partially miscible in PCL/CA ultrafine fibers. The fiber morphology under field emission scanning electron microscopy (FE-SEM) showed that the electrospun ultrafine fibers were bead free. The crystallinity of PCL-CEL, (1:4) blend was greatly decreased in comparison to the treated PCL as revealed by wide angle X-ray diffraction (WAXD) measurements. The potential applications of PCL/CEL webs include liquid biofilters, biosensor and biomedical materials.