Synthesis of germanosilicate type CDS-1 zeolite with CDO topology and its zeolitic layered precursor

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• 作者：Tomoyuki Murase ; Kenichi Komura
• 关键词：Germanosilicate ; CDS ; 1 zeolite ; PLS ; 1 ; Kanemite ; Layered silicate
• 刊名：Journal of Porous Materials
• 出版年：2016
• 出版时间：February 2016
• 年：2016
• 卷：23
• 期：1
• 页码：11-17
• 全文大小：2,417 KB
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• 作者单位：Tomoyuki Murase (1)
  Kenichi Komura (1)
  
  1. Department of Materials Science and Technology, Faculty of Engineering, Gifu University, Gifu City, 501-1193, Japan
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Characterization and Evaluation Materials
  Physical Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1573-4854

文摘

Layered germanosilicate crystalline of PLS-1 (designated as [Ge]PLS-1) is successfully synthesized from the mixture of an acidified kanemite (H-kanemite) and germanium oxide in the presence of tetramethylammonium hydroxide as an organic structure-directing agent. The amount of the installed germanium in the PLS-1 framework can be tunable in the range of Si/Ge ratio from 25 to 200. The topotactic dehydrative condensation process of interlayer’s Q 3 silanol of [Ge]PLS-1 is subjected to yield the corresponding [Ge]CDS-1 zeolite bearing reasonable microporosity. The obtained [Ge]PLS-1 and [Ge]CDS-1 zeolite were characterized by powder-XRD, solid-state NMR, FE-SEM, TG–DTA and N₂ adsorption. Keywords Germanosilicate CDS-1 zeolite PLS-1 Kanemite Layered silicate