Synthesis and characterization of nanocomposite MCM-48-PEHA-DEA and its application as CO2 adsorbent

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• 作者：Mansoor Anbia (1)
  Vahid Hoseini (1)
  Sakineh Mandegarzad (1)
  
• 关键词：CO2 Adsorption ; Nanocomposite ; MCM ; 48 ; Amine Modified
• 刊名：Korean Journal of Chemical Engineering
• 出版年：2012
• 出版时间：December 2012
• 年：2012
• 卷：29
• 期：12
• 页码：1776-1781
• 全文大小：423KB
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• 作者单位：Mansoor Anbia (1)
  Vahid Hoseini (1)
  Sakineh Mandegarzad (1)
  
  1. Research Laboratory of Nanoporous Materials, Faculty of Chemistry, Iran University of Science and Technology, Farjam Street, Narmak, Tehran, 16846, Iran
  
• ISSN：1975-7220

文摘

Three nanocomposites containing MCM-48-35PEHA-15DEA (35 and 15 as weight percent of amine addition), MCM-48-30PEHA-20DEA and MCM-48-25PEHA-25DEA of mesoporous silica MCM-48 modified by the mixture of pentaethylenehexamine (PEHA) and diethanolamine (DEA) have been synthesized and used to study the adsorption of carbon dioxide (CO2). They are characterized by low angle x-ray diffraction (XRD), Fourier transform infrared (FT-IR) and Brunauer-Emmet-Teller (BET) analysis. MCM-48-35PEHA-15DEA (as optimized adsorbent) shows CO2 adsorption capacity of 0.51 (m路mol CO2/g-adsorbent) at 1 bar and 298 K, much higher than CO2 adsorption capacity on polyethyleneimine, pyrrolidinepropyl and polymerized aminopropyl loaded MCM-48.