Selective determination of trace bisphenol a using molecularly imprinted silica nanoparticles containing quenchable fluorescent silver nanoclusters

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• 作者：Chun Deng ; Yaping Zhong ; Yu He ; Yili Ge ; Gongwu Song
• 关键词：Molecular imprint ; Silver nanoclusters ; Fluorescence ; Quenching ; Milk analysis
• 刊名：Microchimica Acta
• 出版年：2016
• 出版时间：January 2016
• 年：2016
• 卷：183
• 期：1
• 页码：431-439
• 全文大小：2,101 KB
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• 作者单位：Chun Deng (2)
  Yaping Zhong (2)
  Yu He (1) (2)
  Yili Ge (1) (2)
  Gongwu Song (1) (2)
  
  2. Ministry-of-Education Key Laboratory for the Synthesis and Application of Organic Functional Molecules, College of Chemistry and Chemical Engineering, Hubei University, Wuhan, 430062, China
  1. Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan, 430062, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Inorganic Chemistry
  Physical Chemistry
  Characterization and Evaluation Materials
  Monitoring, Environmental Analysis and Environmental Ecotoxicology
  
• 出版者：Springer Wien
• ISSN：1436-5073

文摘

We describe a kind of molecularly imprinted polymer (MIP)-based fluorescent sensor. It was obtained by anchoring a surface-imprinted MIP layer for the model analyte bisphenol A (BPA) onto the surface of fluorescent silver nanoclusters (Ag-NCs). The MIP-coated Ag-NCs were synthesized by the sol-gel technique. The hyphenation of the fluorescence of Ag-NCs with MIP technology expands the use of fluorescent nanomaterials in sensing and recognition. BPA is capable of quenching the fluorescence of the Ag-NCs, and the reduction in fluorescence intensity is related to the concentration of BPA in the 0.2 μg mL−1 to 2 mg L−1 range. The detection limit for BPA is 0.02 μg mL−1, and the recovery of BPA from spiked milk and juice samples ranged from 92.5 to 108.5 %. The MIP-coated Ag-NCs presented here are characterized by their ease of synthesis, selectivity and sensitivity. In our perception, this approach can be extended to numerous other analytes.