Preparation and Application of Chitosan-Grafted Multiwalled Carbon Nanotubes in Matrix Solid-Phase Dispersion Extraction for Determination of Trace Acrylamide in Foods Through High-Performance Liquid Chromatography

详细信息    查看全文

• 作者：Handong Zhao ; Ningyang Li ; Jinwang Li ; Xuguang Qiao ; Zhixiang Xu
• 关键词：Acrylamide ; Chitosan ; grafted multiwalled carbon nanotubes ; Matrix solid ; phase dispersion extraction ; High ; performance liquid chromatography
• 刊名：Food Analytical Methods
• 出版年：2015
• 出版时间：May 2015
• 年：2015
• 卷：8
• 期：5
• 页码：1363-1371
• 全文大小：555 KB
• 参考文献：1. Arisseto, AP, Figueiredo Toledo, MCF, Govaert, Y, Loco, J, Fraselle, S, Degroodt, JM (2008) A modified sample preparation for acrylamide determination in cocoa and coffee products. Food Anal Method 1: pp. 49-55 CrossRef
  2. Bacsa, RR, Laurent, C, Peigney, A, Bacsa, WS, Vaugien, T, Rousset, A (2000) High specific surface area carbon nanotubes from catalytic chemical vapor deposition process. Chem Phys Lett 323: pp. 566-571 CrossRef
  3. Barker, SA (2007) Matrix solid dispersion (MSPD). J Biochem Biophys Methods 70: pp. 151-162 CrossRef
  4. Bogialli, S, Corcia, A (2007) Matrix solid-phase dispersion as a valuable tool for extracting contaminants from foodstuffs. J Biochem Biophys Methods 70: pp. 163-179 CrossRef
  5. Casella, IG, Pierri, M, Contursi, M (2006) Determination of acrylamide and acrylic acid by isocratic liquid chromatography with pulsed electrochemical detection. J Chromatogr A 1107: pp. 198-203 CrossRef
  6. Chatterjee, S, Woo, SH (2009) The removal of nitrate from aqueous solutions by chitosan hydrogel beads. J Hazard Mater 164: pp. 1012-1018 CrossRef
  7. Costa, LG, Deng, H, Gregotti, C, Manzo, L, Faustman, EM, Bergmark, E, Calleman, CJ (1991) Comparative studies on the neuro-and reproductive toxicity of acrylamide and its epoxide metabolite glycidamide in the rat. Neurotoxicology 13: pp. 219-224
  8. Dai, BY, Cao, MR, Fang, GZ, Liu, B, Dong, X, Pan, MF, Wang, S (2012) Schiff base-chitosan grafted multiwalled carbon nanotubes as a novel solid-phase extraction adsorbent for determination of heavy metal by ICP-MS. J Hazard Mater 219: pp. 103-110 CrossRef
  9. Fernandes, JO, Soares, C (2007) Application of matrix solid-phase dispersion in the determination of acrylamide in potato chips. J Chromatogr A 1175: pp. 1-6 CrossRef
  10. Gao, ZM, Bandosz, TJ, Zhao, ZB, Han, M, Qiu, JS (2009) Investigation of factors affecting adsorption of transition metals on oxidized carbon nanotubes. J Hazard Mater 167: pp. 357-365 CrossRef
  11. Hernández-Ferrer, J, Laporta, P, Gutiérrez, F, Rubianes, MD, Rivas, G, Martínez, MT (2014) Multi-walled carbon nanotubes/graphene nanoribbons hybrid materials with superior electrochemical performance. J Electrochem Soc 39: pp. 26-29
  Monographs on the evaluation of carcinogenic risk of chemicals to humans. IARC, Lyon
  12. Iijima, S (1991) Helical microtubules of graphitic carbon. Nature 354: pp. 56-58 CrossRef
  13. Kim, SH, Hwang, JH, Lee, KG (2011) Analysis of acrylamide using gas chromatography-nitrogen phosphorus detector (GC-NPD). Food Sci Biotechnol 20: pp. 835-839 CrossRef
  14. Kristenson, EM, Brinkman, UAT, Ramos, L (2006) Recent advances in matrix solid-phase dispersion. TrAC Trends Anal Chem 25: pp. 96-111 CrossRef
  15. Kumar, MNVR (2000) Nano and microparticles as controlled drug delivery devices. J Pharm Sci 3: pp. 234-258
  16. Li, YH, Wang, SG, Wei, JQ, Zhang, X, Xu, C, Luan, ZK, Wei, BQ (2002) Lead adsorption on carbon nanotubes. Chem Phys Lett 357: pp. 263-266 CrossRef
  17. Li, L, Huang, YM, Wang, Y, Wang, WD (2009) Hemimicelle capped functionalized carbon nanotubes-based nanosized solid-phase extraction of arsenic from environmental water samples. Anal Chim Acta 631: pp. 182-188 CrossRef
  18. Liang,
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

In this study, chitosan-grafted multiwalled carbon nanotubes were synthesized and characterized using Fourier transform infrared spectroscopy, transmission electron microscopy, X-ray diffraction, thermogravimetric analysis, and static and kinetic adsorption experiments. The results showed that the resulting material had good adsorption abilities and rapid dynamic properties for acrylamide. This material was used as a sorbent for development of matrix solid-phase dispersion extraction coupled with high-performance liquid chromatography for the determination of trace acrylamide in foods. Under the optimal conditions, the limit of detection, based on three times the signal to noise ratio of the baseline near the analyte peak, was 1.5?μg/L, and the relative standard deviation for five replicate extractions of 50?μg/L acrylamide was 4.3?%. Blank potato and flour samples spiked with acrylamide at different levels, namely, 2.25, 4.50, and 6.75?μg/kg, were extracted and determined by the developed method, with good recoveries ranging from 85.3 to 94.6?%. This method was used for quantitative analysis of acrylamide in different food samples, including twisted cruller, potato chip, and toast samples. Compared with other methods, this method for the extraction and determination of trace acrylamide in food samples is rapid and simple.