One-step synthesis of conductive ceria/polypyrrole nanocomposite particles via photo-induced polymerization method
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- 作者：Hamid Reza Heydarnezhad ; Behzad Pourabbas
- 刊名：Journal of Materials Science: Materials in Electronics
- 出版年：2013
- 出版时间：November 2013
- 年：2013
- 卷：24
- 期：11
- 页码：4378-4385
- 全文大小：594KB
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Behzad Pourabbas (1)
1. Department of Polymer Engineering, Nanostructured Materials Research Center, Sahand University of Technology, 51335-1996, Tabriz, Iran - ISSN：1573-482X
文摘
Inorganic–organic nanocomposites of ceria/polypyrrole with core/shell morphology and median diameter about of 150?nm in single nanoparticles were synthesized by a novel one-step photo-polymerization method using cerium (III) nitrate hexahydrate dissolved in acetonitrile and irradiation under UV wavelengths for 2?h. The photo-polymerization products were characterized using high resolution transmission electron microscopy, Fourier-transform infrared spectroscopy, energy-dispersive X-ray spectroscopy, wide-angle X-ray diffraction, particle size analysis, and field emission scanning electron microscope. Crystalline/amorphous structure was detected for the obtained core/shell nanoparticles via selected area electron diffraction pattern. Electrical conductivity of the nanoparticles was measured by four-probe technique.