Determination of 6-Benzylaminopurine and Hg2+ in Bean Sprouts and Drinking Mineral Water by Surface-Enhanced Raman Spectroscopy

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• 作者：Di Wang ; Fanghui Liang ; Pinyi Ma ; Qingqing Yang ; Dejiang Gao…
• 关键词：6 ; Benzylaminopurine (6 ; BA) ; Hg2+ ; Surface ; enhanced Raman spectroscopy (SERS) ; Bean sprout ; Drinking mineral water
• 刊名：Food Analytical Methods
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：9
• 期：4
• 页码：934-941
• 全文大小：984 KB
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• 作者单位：Di Wang (1)
  Fanghui Liang (2)
  Pinyi Ma (1)
  Qingqing Yang (1)
  Dejiang Gao (3)
  Daqian Song (1)
  Xinghua Wang (1)
  
  1. College of Chemistry, Jilin University, Qianjin Street 2699, Changchun, 130012, People’s Republic of China
  2. Department of Pharmacy, Changchun Medical College, Jilin Street 6177, Changchun, 130031, People’s Republic of China
  3. Changchun Jilin University Little Swan Instruments Co., Ltd., Chuangxin Road 1203, Changchun, 130012, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

A novel method for the determination of 6-benzyladenine (6-BA) in bean sprouts and Hg2+ in drinking mineral water by surface-enhanced Raman spectroscopy (SERS) was described. 6-BA exhibits obvious SERS signal by using the substrate of silver nanoparticles (AgNPs), and the presence of Hg2+ could cause the decrease of SERS signal of 6-BA. The effects of type of aggregation agent, type and level of pH buffer solution, amount of AgNPs, mixing time, concentration of 6-BA, and reaction time on the SERS signals were investigated. Under the optimized experimental conditions, good linear responses were obtained for 6-BA and Hg2+ in the concentration ranges of 10–200 μg L−1 and 5–200 μg L−1, respectively. By the present method, the limits of detection (LODs) for the determination of 6-BA and Hg2+ are 3.3 and 0.20 μg L−1, and the recoveries of 6-BA and Hg2+ in spiked samples are 85.5–113.0 % and 98.2–111.5 %, respectively.