Glucomannan-mediated facile synthesis of gold nanoparticles for catalytic reduction of 4-nitrophenol

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• 作者：Zhao Gao (4)
  Rongxin Su (4) (6)
  Renliang Huang (5)
  Wei Qi (4) (6)
  Zhimin He (4)
  
  4. State Key Laboratory of Chemical Engineering ; School of Chemical Engineering and Technology ; Tianjin University ; Tianjin ; 300072 ; People鈥檚 Republic of China
  6. Collaborative Innovation Center of Chemical Science and Engineering (Tianjin) ; Tianjin ; 300072 ; People鈥檚 Republic of China
  5. School of Environmental Science and Engineering ; Tianjin University ; Tianjin ; 300072 ; People鈥檚 Republic of China
  
• 关键词：Gold nanoparticles ; Catalysis ; Composites ; Glucomannan ; 4 ; Nitrophenol
• 刊名：Nanoscale Research Letters
• 出版年：2014
• 出版时间：December 2014
• 年：2014
• 卷：9
• 期：1
• 全文大小：1,256 KB
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• 刊物主题：Nanotechnology; Nanotechnology and Microengineering; Nanoscale Science and Technology; Nanochemistry; Molecular Medicine;
• 出版者：Springer US
• ISSN：1556-276X

文摘

A facile one-pot approach for synthesis of gold nanoparticles with narrow size distribution and good stability was presented by reducing chloroauric acid with a polysaccharide, konjac glucomannan (KGM) in alkaline solution, which is green and economically viable. Here, KGM served both as reducing agent and stabilizer. The effects of KGM on the formation and stabilization of as-synthesized gold nanoparticles were studied systematically by a combination of UV-visible (UV-vis) absorption spectroscopy, transmission electron microscopy, X-ray diffraction, dynamic light scattering, and Fourier transform infrared spectroscopy. Furthermore, the gold nanoparticles exhibited a notable catalytic activity toward the reduction of 4-nitrophenol to 4-aminophenol.