Solid phase extraction of bisphenol A using magnetic core-shell (Fe3O4@SiO2) nanoparticles coated with an ionic liquid, and its quantitation by HPLC
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- 作者：Songqing Chen ; Jieping Chen ; Xiashi Zhu
- 关键词：Microextraction ; Extraction kinetics ; Magnetic nanomaterial ; Magnetometry ; FTIR ; Fluorescnece ; Quantum yield
- 刊名：Microchimica Acta
- 出版年：2016
- 出版时间：April 2016
- 年：2016
- 卷：183
- 期：4
- 页码：1315-1321
- 全文大小：426 KB
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Jieping Chen (1)
Xiashi Zhu (1)
1. College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou, 225002, People’s Republic of China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Analytical Chemistry
Inorganic Chemistry
Physical Chemistry
Characterization and Evaluation Materials
Monitoring, Environmental Analysis and Environmental Ecotoxicology - 出版者：Springer Wien
- ISSN：1436-5073
文摘
Core-shell nanoparticles (NPs) of the type Fe3O4@SiO2 were prepared, coated with 3 different ionic liquids, and tested for their capability of extracting bisphenol A (BPA). The results showed BPA is best extracted by NPs of the type Fe3O4@SiO2@[OMIM] (where OMIM stands for 1-octyl-3-methylimidazole hexafluorophosphate). Following desorption with methanol, BPA was quantified by HPLC with fluorescence detection in the UV. The following figures of merit were found under optimal conditions: A linear range from 0.5 to 2.0 × 104 μg·L‾1, a detection limit of 90 ng·L‾1, a relative standard deviation of 1.2 % (for n = 3 and 10 μg·L‾1), and a pre-concentration factor of 25. The NPs can be re-used up to 10 times. The method was successfully applied to the determination of BPA in plastic tableware.