Certification of reference materials for the determination of alkylphenols

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• 作者：Nobuyasu Hanari (1)
  Keiichiro Ishikawa (1)
  Yoshitaka Shimizu (1)
  Satoko Otsuka (1)
  Ryoko Iwasawa (1)
  Naomi Fujiki (1)
  Masahiko Numata (1)
  Takashi Yarita (1)
  Kenji Kato (1)
  
  1. National Metrology Institute of Japan (NMIJ) ; National Institute of Advanced Industrial Science and Technology (AIST) ; 1-1-1 ; Umezono ; Tsukuba ; Ibaraki ; 305-8563 ; Japan
  
• 关键词：Certified reference material ; Endocrine disrupter ; Alkylphenol ; Japan Calibration Service System ; Traceability
• 刊名：Analytical and Bioanalytical Chemistry
• 出版年：2015
• 出版时间：April 2015
• 年：2015
• 卷：407
• 期：11
• 页码：3239-3247
• 全文大小：355 KB
• 参考文献：1. Khim, JS, Villeneuve, DL, Kannan, K, Lee, KT, Snyder, SA, Koh, CH, Giesy, JP (1999) Alkylphenols, polycyclic aromatic hydrocarbons, and organochlorines in sediment from Lake Shihwa, Korea: instrumental and bioanalytical characterization. Environ Toxicol Chem 18: pp. 2424-2432
  2. Environment Canada Health Canada (2000) Nonylphenol and its ethoxylates (Priority Substances List Assessment Report). Available at: http://dsp-psd.pwgsc.gc.ca/Collection/En40-215-57E.pdf. Accessed 13 Nov 2014
  3. Jobling, S, Sumpter, JP (1993) Detergent components in sewage effluent are weakly estrogenic to fish: an in-vitro study using rainbow-trout (Oncorhynchus mykiss) hepatocytes. Aquat Toxicol 27: pp. 361-372 CrossRef
  4. Information on the Japan Calibration Service System (JCSS). Available at: http://www.iajapan.nite.go.jp/jcss/en/index.html. Accessed 13 Nov 2014
  5. Miyata Y, Shikakume K (2003) Chem Times 4:2鈥? in Japanese. Available at: http://www.kanto.co.jp/times/pdf/CT_190_all.pdf. Accessed 13 Nov 2014
  6. Information on designated calibration body based on the Japan Calibration Service System (JCSS). Available http://www.cerij.or.jp/ceri_en/index_e4.shtml. Accessed 13 Nov 2014
  7. Hanari, N, Ishikawa, K, Shimizu, Y, Iwasawa, R, Otsuka, S, Fujiki, N, Bao, X, Yarita, T, Kato, K, Yamashita, N (2009) Certified reference materials for determination of phthalates and alkylphenols form the National Metrology Institute of Japan. Organohalogen Compd 71: pp. 1605-1609
  8. Hanari, N, Iwasawa, R, Otsuka, S, Fujiki, N, Matsumoto, A, Ihara, T, Ishikawa, K, Yarita, T (2010) Water content variation of p-n-heptylphenol reference material. Accredit Qual Assur 15: pp. 673-679 CrossRef
  9. Ishikawa, K, Hanari, N, Shimizu, Y, Ihara, T, Nomura, A, Numata, M, Yarita, T, Kato, K, Chiba, K (2011) Mass balance method for purity assay of phthalic acid esters: development of primary reference materials as traceability sources in the Japan Calibration Service System. Accredit Qual Assur 16: pp. 311-322 CrossRef
  10. Shimizu, Y, Ohte, Y, Bao, X, Otsuka, S, Kitamaki, Y, Ishikawa, K, Ihara, T, Kato, K (2008) Development of certified reference materials of high-purity volatile organic compounds: purity assay by the freezing-point depression method. Accredit Qual Assur 13: pp. 389-396 CrossRef
  11. Milton, MJT, Quinn, TJ (2001) Primary methods for the measurement of amount of substance. Metrologia 38: pp. 289-296 CrossRef
  JIS K 0450-10-10: testing method for bisphenol A in industrial water and waste water. Japanese Standards Association Publication, Tokyo
  JIS K 0450-20-10: testing method for alkyl phenols in industrial water and wastewater. Japanese Standards Association Publication, Tokyo
  12. van Dooren AA, Muller BW (1984) Purity determinations of drugs with differential scanning calorimetry (DSC) - a critical review. Int J Pharm 20:217鈥?33
  13. Mraw, SC (1982) Mathematical treatment of heat-flow in differential scanning calorimetry and differential thermal-analysis instruments. Rev Sci Instrum 53: pp. 228-231 CrossRef
  14. Saito, Y, Saito, K, Atake, T (1986) Theoretical-analysis of heat-flux differential scanning calorimetry based on a general-model. Thermochim Acta 99: pp. 299-307 CrossRef
  ISO 6142: gas analysis 鈥?preparation of calibration gas mixtures 鈥?gravimetric method. ISO Publication, Geneva
  15. Hanari, N, Ishikawa, K, Otsuka, S, Higuchi, K, Iwasawa, R, Yarita, T (2008) Certified calibration solution reference material for the determination of benzo[a]pyrene from the National Metrology Institute of Japan (NMIJ). Polycycl Aromat Comp 28: pp. 302-319 CrossRef
  16. Nesterova, TN, Nazmutdinov, AG, Tsvetkov, VS, Rozhnov, AM, Yu Roshchupkina, I (1990) Vapor-pressures and enthalpies of vaporization of alkylphenols. J Chem Thermodyn 22: pp. 365-377 CrossRef
  17. Verevkin, SP (1999) Thermochemistry of phenols: quantification of the ortho, para-, and meta-interactions in tert-alkyl substituted phenols. J Chem Thermodyn 31: pp. 559-585 CrossRef
  Guide to the expression of uncertainty in measurement. ISO Publication, Geneva
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  ISO/IEC 17025: general requirements for the competence of testing and calibration laboratories. ISO Publication, Geneva
  18. Hanari, N, Ishikawa, K, Yarita, T, Otsuka, S, Iwasawa, R, Fujiki, N, Numata, M (2011) Purity evaluation of alkylphenol primary standards based on Japan Calibration Service System by subtraction method. Bunseki Kagaku 60: pp. 877-884 CrossRef
  19. Coplen, TB, Peiser, HS (1998) History of the recommended atomic-weight values from 1882 to 1997: a comparison of differences from current values to the estimated uncertainties of earlier values. Pure Appl Chem 70: pp. 237-257 CrossRef
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  21. Ihara, T, Iijima, Y, Shimizu, Y (2008) Uncertainty evaluation for purity analysis of organochlorine compounds by freezing-point depression method using differential scanning calorimeter. Bunseki Kagaku 57: pp. 493-498 CrossRef
  22. NIST (2012) Certificate of analysis. SRM 1584: Priority Pollutant Phenols in Methanol. National Institute of Standards and Technology: Gaithersburg
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Analytical Chemistry
  Food Science
  Inorganic Chemistry
  Physical Chemistry
  Monitoring, Environmental Analysis and Environmental Ecotoxicology
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1618-2650

文摘

Certified reference materials (CRMs) are playing an increasingly important role in national and international standardizing activities. In Japan, primary standard solutions for analyses of endocrine disrupters are supplied under the national standards dissemination system named the Japan Calibration Service System (JCSS). For the traceability on reference materials used for preparation of the primary standard solutions based on the JCSS, the National Metrology Institute of Japan, National Institute of Advanced Industrial Science and Technology (NMIJ/AIST) has developed and certified high-purity reference materials of alkylphenols as NMIJ CRMs, such as 4-n-nonylphenol, 4-tert-octylphenol, 4-n-heptylphenol, 4-tert-butylphenol, and 2,4-dichlorophenol. Thereafter, it is essential to determine the alkylphenols by using these solutions based on the JCSS for environmental monitoring and risk assessments because analytical values obtained by using the solutions can ensure the reliability and traceability of the chemical analyses.