Two New Zn(II)/Cd(II) Coordination Polymers Based on Rigid Squaric Acid: Crystal Structure, Topology and Fluorescent Properties

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• 作者：Ping Tang ; Wen-Wen Dong ; Wei Xia ; Jun Zhao
• 关键词：Squaric acid ; Coordination polymer ; Network topology ; Fluorescent property
• 刊名：Journal of Inorganic and Organometallic Polymers and Materials
• 出版年：2015
• 出版时间：May 2015
• 年：2015
• 卷：25
• 期：3
• 页码：569-575
• 全文大小：1,096 KB
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• 作者单位：Ping Tang (1)
  Wen-Wen Dong (2)
  Wei Xia (1)
  Jun Zhao (2)
  
  1. College of Biological and Pharmaceutical Sciences, China Three Gorges University, Yichang, 443002, People’s Republic of China
  2. College of Materials and Chemical Engineering, China Three Gorges University, Yichang, 443002, People’s Republic of China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Inorganic Chemistry
  Organic Chemistry
  Polymer Sciences
  
• 出版者：Springer New York
• ISSN：1574-1451

文摘

Presented here are two d10 metal–organic coordination polymers (CPs), [Zn(C₄O₄)_0.5(μ ₃-OH)] _n (1) and [Cd(C₄O₄)_0.5(OX)_0.5(H₂O)] _n (2) (H₂OX?=?oxalic acid) constructed from squaric acid (H₂C₄O₄) tectons. Single-crystal X-ray diffraction studies indicated that both 1 and 2 show 3D structures. The two 3D CPs are assembled from 1D {[Zn(μ ₃-OH)] _n + } chains to 3D structure linked through C₄O₄ 2?/sup> ligands for 1 and 2D {[(Cd1)₂(C₄O₄)]2+} layers pillared by OX2?/sup> ligands for 2. The structure of compound 1 can be described as a trinodal (3,6,6)-connected net with the point symbol of {43}₂{44·610·8}{45·610}₂, whereas 2 possess a trinodal (4,5,6)-connected {42·84} {46·66·83} {48·62}₂ topology. Furthermore, the fluorescent and thermal stabilities properties of these two compounds were investigated.