Mechanical properties and crystallization behavior of poly(butylene succinate) composites reinforced with basalt fiber

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• 作者：Yi Li ; Lin Sang ; Zhiyong Wei ; Chen Ding…
• 关键词：Poly(butylene succinate) ; Basalt fiber ; Morphology ; Mechanical properties ; Thermal properties
• 刊名：Journal of Thermal Analysis and Calorimetry
• 出版年：2015
• 出版时间：October 2015
• 年：2015
• 卷：122
• 期：1
• 页码：261-270
• 全文大小：2,043 KB
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• 作者单位：Yi Li (1)
  Lin Sang (2)
  Zhiyong Wei (3)
  Chen Ding (2)
  Ying Chang (2)
  Guangyi Chen (2)
  Wanxi Zhang (2)
  Jicai Liang (1) (2)
  
  1. Key Laboratory of Automotive Materials, Ministry of Education and College of Materials Science and Engineering, Jilin University, Changchun, 130025, China
  2. State Key Laboratory of Structural Analysis for Industrial Equipment and School of Automotive Engineering, Dalian University of Technology, Dalian, 116024, China
  3. Department of Polymer Science and Materials, School of Chemical Engineering, Dalian University of Technology, Dalian, 116024, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Sciences
  Polymer Sciences
  Physical Chemistry
  Inorganic Chemistry
  Measurement Science and Instrumentation
  
• 出版者：Akad茅miai Kiad贸, co-published with Springer Science+Business Media B.V., Formerly Kluwer Academic
• ISSN：1572-8943

文摘

Biodegradable poly(butylene succinate) (PBS)/basalt fiber (BF) composites were prepared by melt blending method using twin-screw extruder followed by injection molding. Mechanical properties, crystallization and melting behavior, morphology, crystal structure and thermal stability of PBS/BF composites with various BF contents were investigated by different techniques. The tensile and impact properties of the composites were improved markedly with the addition of BF, due to the efficient interfacial adhesion between fibers and PBS matrix. Crystallization and melting behavior of PBS in its composites kept almost unchanged, indicating that the nucleation effect of BF was minimal and, meanwhile, it played a role in hindrance of chain motion. TG analysis showed that the thermal stability of PBS/BF composites was enhanced by the addition of BF. The crystal structure of PBS was not affected by the incorporation of BF, while the nucleation density increased gradually and the spherulite size reduced remarkably with the increase in BF. No transcrystallization phenomenon on the surface of BF was observed maybe as a result of without surface treatment. Keywords Poly(butylene succinate) Basalt fiber Morphology Mechanical properties Thermal properties