Synthesis of p-aminophenol from p-nitrophenol reduction over Pd@ZIF-8
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- 作者：Hong Jiang ; Qing Yan ; Yan Du ; Rizhi Chen
- 关键词：p ; Aminophenol ; p ; Nitrophenol reduction ; Zeolitic imidazolate frameworks ; Palladium nanoparticles ; Polyvinylpyrrolidone
- 刊名：Reaction Kinetics, Mechanisms and Catalysis
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：117
- 期：1
- 页码：307-317
- 全文大小：736 KB
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Qing Yan (1)
Yan Du (2)
Rizhi Chen (1)
1. State Key Laboratory of Materials-Oriented Chemical Engineering, Nanjing Tech University, Nanjing, Jiangsu, 210009, China
2. College of Environment, Nanjing Tech University, Nanjing, Jiangsu, 210009, China - 刊物类别：Chemistry and Materials Science
- 刊物主题：Chemistry
Catalysis
Industrial Chemistry and Chemical Engineering
Physical Chemistry - 出版者：Akad茅miai Kiad贸, co-published with Springer Science+Business Media B.V., Formerly Kluwer Academic
- ISSN：1878-5204
文摘
p-Aminophenol was synthesized by the catalytic reduction of p-nitrophenol over Pd@ZIF-8 prepared by an assembly method that involves the construction of ZIF-8 crystals around the pre-synthesized polyvinylpyrrolidone (PVP)-stabilized palladium nanoparticles. The catalyst was characterized in detail by XRD, FESEM, HRTEM, XPS, ICP, N2 sorption, TGA and FT-IR. The analysis results show that the hybrid material Pd@ZIF-8 has a rhombic dodecahedral structure like ZIF-8, the particle size of Pd@ZIF-8 is about 400 nm, which is much greater than that of ZIF-8 due to the promotion of PVP, and the pre-synthesized Pd nanoparticle with a diameter of 2–5 nm can be well dispersed within the ZIF-8 crystals. The as-prepared Pd@ZIF-8 catalyst exhibits much higher catalytic activity than the commercial Raney Ni in the reduction of p-nitrophenol to p-aminophenol, and can be reused at least five times without obvious loss in catalytic activity. Furthermore, the Pd@ZIF-8 shows outstanding catalytic selectivity for the synthesis of p-aminophenol, and only target product p-aminophenol is formed in the p-nitrophenol reduction. The better catalytic performance of Pd@ZIF-8 may be caused by the small size and high dispersion of Pd nanoparticles confined within the ZIF-8 framework. Keywords p-Aminophenol p-Nitrophenol reduction Zeolitic imidazolate frameworks Palladium nanoparticles Polyvinylpyrrolidone