Hydrothermal synthesis of a new zinc phosphite (C5H7N2)2·[Zn3(HPO3)4] with intersecting 8- and 12-ring channels

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• 作者：Zhaojun Dong ; Yan Yan ; Wenqing Zhang ; Yu Wang…
• 关键词：Hydrothermal synthesis ; Zinc phosphite ; Open framework ; Photoluminescence
• 刊名：Chemical Research in Chinese Universities
• 出版年：2015
• 出版时间：August 2015
• 年：2015
• 卷：31
• 期：4
• 页码：498-502
• 全文大小：645 KB
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• 作者单位：Zhaojun Dong (1) (2)
  Yan Yan (2)
  Wenqing Zhang (1)
  Yu Wang (1)
  Jiyang Li (2)
  
  1. Key Lab of Groundwater Resources and Environment, Ministry of Education, College of Environment and Resources, Jilin University, Changchun, 130021, P. R. China
  2. State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry, Jilin University, Changchun, 130012, P. R. China
  
• 刊物主题：Chemistry/Food Science, general; Analytical Chemistry; Inorganic Chemistry; Organic Chemistry; Physical Chemistry;
• 出版者：Springer Berlin Heidelberg
• ISSN：2210-3171

文摘

Using 4-aminopyridine as the structure-directing agent(SDA), a new open-framework zinc phosphite, (C5H7N2)2·[Zn3(HPO3)4](ZnHPO-CJ70), was synthesized under hydrothermal condition. Single-crystal X-ray diffraction analysis reveals that ZnHPO-CJ70 is constructed by the strictly alternating ZnO4 tetrahedra and HPO3 pseudo-pyramids, with their vertexes linked to generate a three-dimensional(3D) open framework with intersecting 8- and 12-ring channels. Further characterizations of ZnHPO-CJ70 were performed by means of X-ray powder diffraction(XRD), elemental analysis(ICP, CHN), infrared spectroscopy(IR) and thermogravimetric(TG) analyses. The results of luminescent test shows that ZnHPO-CJ70 exhibits strong fluorescence emissions in the solid state at room temperature.