同位素比质谱技术在食品应用中的研究进展
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摘要
同位素比质谱技术在很多领域已有广泛的应用,尤其是食品质量真伪鉴别方面,国际上已经取得了一系列研究成果。综述同位素比质谱技术在葡萄酒、蜂蜜、肉类、植物油、果汁及调味品等各类食品掺假鉴别及原材料的产地溯源等方面的应用,以期为管理部门的监管、生产厂家的质量控制提供参考。
Isotope ratio mass spectrometry has been widely used in many fields,especially in the field of food quality,which has achieved a series of research results in the world.The application of isotope ratio mass spectrometry was reviewed in identifing the authenticity and traceability of raw materials of various kinds of foods(such as wine,honey,meat,vegetable oil,fruit juice and flavouring,etc.)with the purpose of providing theoretical basis for the supervision of the management department and the quality control of manufacturer.
Isotope ratio mass spectrometry has been widely used in many fields,especially in the field of food quality,which has achieved a series of research results in the world.The application of isotope ratio mass spectrometry was reviewed in identifing the authenticity and traceability of raw materials of various kinds of foods(such as wine,honey,meat,vegetable oil,fruit juice and flavouring,etc.)with the purpose of providing theoretical basis for the supervision of the management department and the quality control of manufacturer.
引文
[1]耿安松,熊永强.应用GC-IRMS技术测定气源岩热解产物中轻烃的碳同位素组成[J].科学通报,2000,45(21):2695-2698
[2]于志强,彭平安,傅家谟,等.卟啉化合物碳同位素的气相色谱-同位素比值质谱测定技术[J].色谱,2001,19(2):97-100
[3]杜丽,李立武,孟仟祥,等.甘肃窑街中侏罗世油页岩单体烃碳同位素分析对比研究[J].质谱学报,2005,26(21):55-56
[4]Friedman I,Smith G L,Gleason J D.Stable isotop composition of waters in southeastern California.Modern precipitation[J].Journal of Geophys Research,1992,97(D5):795-812
[5]张琳,韩梅,贾艳琨,等.同位素比值质谱与激光吸收光谱分析水中氢氧同位素方法的比较[J].质谱学报,2015,36(6):559-564
[6]Ferretti D F.A new chromatograph-isotope ratio mass spectrometry technique for high-precision,N2O-free analysis ofδ13C andδ18O in atmospheric CO2from small air samples[J].Geophysical Research,2000,105:6709-6718
[7]刘立新,周凌晞,夏玲君,等.气体稳定同位素比质谱法分析本底大气CO2的δ13C和δ18O[J].环境科学学报,2012,32(6):1299-1305
[8]Rossmann A,Koziet J.Determination of the carbon-13 content of sugars and pulp from fruit juiees by isotope ration 1118~5 spectrometry(intemal roference method)A European interlaboratory eomparision[J].Analytiea Chimiea Aeta,1997(340):21-29
[9]Norman A L,Hopper J F.The stable carbon isotope composition of atmospheric PAHs[J].Atmospheric Envimment,1999(33):2807-2814
[10]Rossmann A.Determination of stable isotope rations in food analysis[J].Food Reviews International,2001,17(3):347-381
[11]White J W,Winters K.Honey protein as internal standard for stable carbon isotope ratio detection of adulteration honey[J].Journal of the Association of Oficial Analytical Chemists,1989,72:907-911
[12]Elflein L,Raezke K P.Improved detection of honey adulteration by measuring diferences between13C/12C stable carbon isotope ratios of protein and sugar compounds with a combination of elemental analyzer-isotope ratio mass spectrometry and liquid chromatographyisotope ratio mass spectrometry(δ13C-EA/LC-IRMS)[J].Apidologie,2008,39(5):574-589
[13]Jarnina E,Gonzaleza J,Remauda G C,et al.Improved detection of sugar addition to apple juices and concentrates using internal standard13C IRMS[J].Analytica Chimica Acta,1997,347:359-368
[14]White J W,Doner L W.Mass spectrometric detection of high-fructose corn syrup by use of the13C/12C ratio:collaborative study[J].J.Assoc.Off.Anal.Chem,1978,61(3):746-750
[15]王鹏.鲍鱼中碳、氮同位素的分析[J].化学分析计量,2013,22(7):14-16
[16]国振,符惠,李秀琴,等.橙汁中苯甲酸含量测定的国际比对APMP.QM-P23[J].色谱,2013,31(12):1194-1200
[17]费晓庆,吴斌,沈崇钰.液相色谱/元素分析-同位素比值质谱联用法鉴定蜂蜜掺假[J].色谱,2011,29(1):15-19
[18]陈文斌,钟其顶,王道兵.气相色谱-同位素质谱(GC-C-IRMWS)测定饮料酒中乙醇13C/12C比值方法研究[J].酿酒科技,2013(5):90-93
[19]刘晓星,唐小华,廉晗熠.碳稳定同位素比质谱法对海上溢油中燃料油及原油的鉴别[J].大连海事大学学报,2014,40(4):109-112
[20]Regulation E C.Detecting enrichment of grape musts,concentrated grape musts,rectified concentrated grape musts and wines by application of nuclear magnetic resonance of deuterium(SNIF-NMR)[R].Official Journal of the European Communities 1990,L272(33):64-73
[21]中国秦皇岛出入境检验检疫局.GB/T 18932.1-2002蜂蜜中碳-4植物糖含量测定方法稳定碳同位素比率法[S].北京:中国标准出版社,2002
[22]中华人民共和国国家质量监督检验检疫总局,SN/T3846-2014出口苹果和浓缩苹果汁中碳同位素比值的测定[S].中国标准出版社,2004
[23]Remaud G,Guillou C,Vallet C,et al.A coupled NMR and MS isotopic method for the authentication of natural vinegars[J].Fresenius Journal of Analytical Chemistry,1992,342(4):457-461
[24]李学民,贾光群,曹彦忠,等.液相色谱-同位素比质谱法同时测定葡萄酒中甘油和乙醇的δ13C值[J].色谱,2013,31(12):1201-1205
[25]李学民,贾光群,王蕾,等.元素分析-同位素比质谱法测定葡萄酒中乙醇δ13C值[J].分析化学研究报告,2014,42(1):99-103
[26]Carola V,Qietrich Von B,Claudia M,et al.Overview of chemical markers for varietal authentication of red wines[M].Washington:American Chemical Society Symposim Series,2011:101-111
[27]江伟,吴幼茹,薛洁.C、H、O同位素分析在葡萄酒产区鉴别中的应用[J].食品科学,2016,37(6):166-171
[28]吴浩,谢丽琪,靳保辉,等.气相色谱-燃烧-同位素比率质谱法测定葡萄酒中5种挥发性组分的碳同位素比值及其在产地溯源中的应用[J].分析化学,2015,43(3):344-349
[29]AOAC Official methods of analysis,12th ed.The content of C4 plant sugar in honey—Internal standard stable carbon isotope ratio method[S].Washington:Association of Official Analytical Chemists:1975
[30]李学民,曹彦忠,贾光群,等.液相色谱-同位素比质谱法测定蜂蜜中糖组分δ13C值[J].中国蜂业,2012,63(21):79-82,87
[31]朱绍华,张帆,王美玲,等.稳定同位素比质谱法鉴别茶油中掺杂玉米油研究[J].中国食物与营养,2013,9(13):8-10
[32]金青哲,谢峰,丁志华,等.花生油和玉米油掺合物的碳同位素比值质谱法检测研究[J].中国粮油学报,2010,25(5):95-98
[33]王修宁,赵超敏,韩丽,等.元素分析-同位素比质谱法测定食醋总碳同位素比值[J].现代食品科技,2016,32(6)
[34]谭梦茹,林宏,沈崇钰,等.元素分析-碳同位素比值质谱法在酿造酱油掺假鉴别中的应用[J].质谱学报,2015,36(4):334-339
[35]李鑫,陈小珍,张东雷,等.元素分析-稳定同位素比质谱同时测定δ13C/δ15N在原料乳检验中的应用[J].分析科学学报,2013,29(3):356-359
[36]梁莉莉,陈剑,侯敬丽,等.元素分析-稳定同位素比质谱技术在婴幼儿配方奶粉奶源地追溯中的应用[J].质谱学报,2015,36(1):66-71
[37]张遴,蔡砚,乐爱山,等.稳定同位素比质谱法鉴别蔗糖和甜菜糖[J].2010,31(2):124-126
[38]张遴,蔡砚,李高华,等.稳定同位素比质谱法测定苹果和浓缩苹果汁的δ13C值[J].理化检验-化学分册,2010,48(1):8-10,14
[39]张遴.中国富士苹果碳同位素比的含量和分布特征[J].食品安全质量检测学报,2013,3(2):501-503
[40]潘明.马铃薯淀粉与玉米淀粉的特性及其应用比较[J].中国马铃薯,2001,15(4):222-226
[41]王绍清,武士奎,穆同娜,等.扫描电镜和稳定碳同位素比质谱法鉴别马铃薯淀粉中的掺假玉米淀粉[J].食品科学,2010,31(20):332-335
[2]于志强,彭平安,傅家谟,等.卟啉化合物碳同位素的气相色谱-同位素比值质谱测定技术[J].色谱,2001,19(2):97-100
[3]杜丽,李立武,孟仟祥,等.甘肃窑街中侏罗世油页岩单体烃碳同位素分析对比研究[J].质谱学报,2005,26(21):55-56
[4]Friedman I,Smith G L,Gleason J D.Stable isotop composition of waters in southeastern California.Modern precipitation[J].Journal of Geophys Research,1992,97(D5):795-812
[5]张琳,韩梅,贾艳琨,等.同位素比值质谱与激光吸收光谱分析水中氢氧同位素方法的比较[J].质谱学报,2015,36(6):559-564
[6]Ferretti D F.A new chromatograph-isotope ratio mass spectrometry technique for high-precision,N2O-free analysis ofδ13C andδ18O in atmospheric CO2from small air samples[J].Geophysical Research,2000,105:6709-6718
[7]刘立新,周凌晞,夏玲君,等.气体稳定同位素比质谱法分析本底大气CO2的δ13C和δ18O[J].环境科学学报,2012,32(6):1299-1305
[8]Rossmann A,Koziet J.Determination of the carbon-13 content of sugars and pulp from fruit juiees by isotope ration 1118~5 spectrometry(intemal roference method)A European interlaboratory eomparision[J].Analytiea Chimiea Aeta,1997(340):21-29
[9]Norman A L,Hopper J F.The stable carbon isotope composition of atmospheric PAHs[J].Atmospheric Envimment,1999(33):2807-2814
[10]Rossmann A.Determination of stable isotope rations in food analysis[J].Food Reviews International,2001,17(3):347-381
[11]White J W,Winters K.Honey protein as internal standard for stable carbon isotope ratio detection of adulteration honey[J].Journal of the Association of Oficial Analytical Chemists,1989,72:907-911
[12]Elflein L,Raezke K P.Improved detection of honey adulteration by measuring diferences between13C/12C stable carbon isotope ratios of protein and sugar compounds with a combination of elemental analyzer-isotope ratio mass spectrometry and liquid chromatographyisotope ratio mass spectrometry(δ13C-EA/LC-IRMS)[J].Apidologie,2008,39(5):574-589
[13]Jarnina E,Gonzaleza J,Remauda G C,et al.Improved detection of sugar addition to apple juices and concentrates using internal standard13C IRMS[J].Analytica Chimica Acta,1997,347:359-368
[14]White J W,Doner L W.Mass spectrometric detection of high-fructose corn syrup by use of the13C/12C ratio:collaborative study[J].J.Assoc.Off.Anal.Chem,1978,61(3):746-750
[15]王鹏.鲍鱼中碳、氮同位素的分析[J].化学分析计量,2013,22(7):14-16
[16]国振,符惠,李秀琴,等.橙汁中苯甲酸含量测定的国际比对APMP.QM-P23[J].色谱,2013,31(12):1194-1200
[17]费晓庆,吴斌,沈崇钰.液相色谱/元素分析-同位素比值质谱联用法鉴定蜂蜜掺假[J].色谱,2011,29(1):15-19
[18]陈文斌,钟其顶,王道兵.气相色谱-同位素质谱(GC-C-IRMWS)测定饮料酒中乙醇13C/12C比值方法研究[J].酿酒科技,2013(5):90-93
[19]刘晓星,唐小华,廉晗熠.碳稳定同位素比质谱法对海上溢油中燃料油及原油的鉴别[J].大连海事大学学报,2014,40(4):109-112
[20]Regulation E C.Detecting enrichment of grape musts,concentrated grape musts,rectified concentrated grape musts and wines by application of nuclear magnetic resonance of deuterium(SNIF-NMR)[R].Official Journal of the European Communities 1990,L272(33):64-73
[21]中国秦皇岛出入境检验检疫局.GB/T 18932.1-2002蜂蜜中碳-4植物糖含量测定方法稳定碳同位素比率法[S].北京:中国标准出版社,2002
[22]中华人民共和国国家质量监督检验检疫总局,SN/T3846-2014出口苹果和浓缩苹果汁中碳同位素比值的测定[S].中国标准出版社,2004
[23]Remaud G,Guillou C,Vallet C,et al.A coupled NMR and MS isotopic method for the authentication of natural vinegars[J].Fresenius Journal of Analytical Chemistry,1992,342(4):457-461
[24]李学民,贾光群,曹彦忠,等.液相色谱-同位素比质谱法同时测定葡萄酒中甘油和乙醇的δ13C值[J].色谱,2013,31(12):1201-1205
[25]李学民,贾光群,王蕾,等.元素分析-同位素比质谱法测定葡萄酒中乙醇δ13C值[J].分析化学研究报告,2014,42(1):99-103
[26]Carola V,Qietrich Von B,Claudia M,et al.Overview of chemical markers for varietal authentication of red wines[M].Washington:American Chemical Society Symposim Series,2011:101-111
[27]江伟,吴幼茹,薛洁.C、H、O同位素分析在葡萄酒产区鉴别中的应用[J].食品科学,2016,37(6):166-171
[28]吴浩,谢丽琪,靳保辉,等.气相色谱-燃烧-同位素比率质谱法测定葡萄酒中5种挥发性组分的碳同位素比值及其在产地溯源中的应用[J].分析化学,2015,43(3):344-349
[29]AOAC Official methods of analysis,12th ed.The content of C4 plant sugar in honey—Internal standard stable carbon isotope ratio method[S].Washington:Association of Official Analytical Chemists:1975
[30]李学民,曹彦忠,贾光群,等.液相色谱-同位素比质谱法测定蜂蜜中糖组分δ13C值[J].中国蜂业,2012,63(21):79-82,87
[31]朱绍华,张帆,王美玲,等.稳定同位素比质谱法鉴别茶油中掺杂玉米油研究[J].中国食物与营养,2013,9(13):8-10
[32]金青哲,谢峰,丁志华,等.花生油和玉米油掺合物的碳同位素比值质谱法检测研究[J].中国粮油学报,2010,25(5):95-98
[33]王修宁,赵超敏,韩丽,等.元素分析-同位素比质谱法测定食醋总碳同位素比值[J].现代食品科技,2016,32(6)
[34]谭梦茹,林宏,沈崇钰,等.元素分析-碳同位素比值质谱法在酿造酱油掺假鉴别中的应用[J].质谱学报,2015,36(4):334-339
[35]李鑫,陈小珍,张东雷,等.元素分析-稳定同位素比质谱同时测定δ13C/δ15N在原料乳检验中的应用[J].分析科学学报,2013,29(3):356-359
[36]梁莉莉,陈剑,侯敬丽,等.元素分析-稳定同位素比质谱技术在婴幼儿配方奶粉奶源地追溯中的应用[J].质谱学报,2015,36(1):66-71
[37]张遴,蔡砚,乐爱山,等.稳定同位素比质谱法鉴别蔗糖和甜菜糖[J].2010,31(2):124-126
[38]张遴,蔡砚,李高华,等.稳定同位素比质谱法测定苹果和浓缩苹果汁的δ13C值[J].理化检验-化学分册,2010,48(1):8-10,14
[39]张遴.中国富士苹果碳同位素比的含量和分布特征[J].食品安全质量检测学报,2013,3(2):501-503
[40]潘明.马铃薯淀粉与玉米淀粉的特性及其应用比较[J].中国马铃薯,2001,15(4):222-226
[41]王绍清,武士奎,穆同娜,等.扫描电镜和稳定碳同位素比质谱法鉴别马铃薯淀粉中的掺假玉米淀粉[J].食品科学,2010,31(20):332-335
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