Rapid screening and quantification of multi-class multi-residue veterinary drugs in royal jelly by ultra performance liquid chromatography coupled to quadrupole time-of-flight mass spectrometry
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- 作者：Yaqian Zhanga ; Xiaomao Liub ; Xiang Lib ; Jinjie Zhangb ; Yanzhong Caob ; Ming Sua ; Zhihong Shia ; Hanwen Suna ; hanwen@hbu.edu.cn" class="auth_mail" title="E-mail the corresponding author
- 关键词：Ultra performance liquid chromatography ; Quadrupole time-of-flight mass spectrometry ; QuEChERS ; Veterinary drug residues ; Royal jelly
- 刊名：Food Control
- 出版年：2016
- 出版时间：February 2016
- 年：2016
- 卷：60
- 期：Complete
- 页码：667-676
- 全文大小：741 K
文摘
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A new screening and quantification method for multi-class multi-residue veterinary drugs was developed.
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A total of 90 veterinary drugs were analyzed by UPLC-QTOF-MS with modified QuEChERS procedure.
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The linearity, sensitivity, accuracy, repeatability, and reproducibility of the method were fully validated.
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A homemade database was established and utilized for the confirmation and identification of the target drugs.
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The method can be used for rapid screening and quantification of the 90 residues in royal jelly samples.
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