On ball-milled ODS ferritic steel recrystallization: From as-milled powder particles to consolidated state

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• 作者：Nicolas Sallez (1) (2)
  Patricia Donnadieu (1) (2)
  Eglantine Courtois-Manara (3)
  Delphine Chassaing (3)
  Christian K眉bel (3)
  Frederic Delabrouille (4)
  Martine Blat-Yrieix (4)
  Yann de Carlan (5)
  Yves Br茅chet (1) (2)
  
  1. Universit茅 Grenoble Alpes ; SIMAP ; 38000 ; Grenoble ; France
  2. CNRS ; SIMAP ; 38000 ; Grenoble ; France
  3. Karlsruhe Nano Micro Facility & Institute of Nanotechnology ; Karlsruhe Institute of Technology ; Hermann-von-Helmhotz-Platz 1 ; 76344 ; Eggenstein-Leopoldshafen ; Germany
  4. EDF 鈥?EDF R&D ; Les Renardi猫res ; 77818 ; Moret-sur-Loing ; France
  5. CEA ; DEN ; Service de Recherches M茅tallurgiques Appliqu茅es ; 91191 ; Gif-sur-Yvette ; France
  
• 刊名：Journal of Materials Science
• 出版年：2015
• 出版时间：March 2015
• 年：2015
• 卷：50
• 期：5
• 页码：2202-2217
• 全文大小：6,287 KB
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• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Materials Science
  Characterization and Evaluation Materials
  Polymer Sciences
  Continuum Mechanics and Mechanics of Materials
  Crystallography
  Mechanics
  
• 出版者：Springer Netherlands
• ISSN：1573-4803

文摘

Recrystallization of a ball-milled ferritic ODS steel is studied towards its evolution from as-milled powder to consolidated state. This characterization has been made possible by using a combination of X-ray Diffraction (XRD) and an innovative method based on an Automated Crystallographic Orientation Mapping (ACOM) tool attached to a Transmission Electron Microscope (TEM). Focus Ion Beam preparation has been essential to obtain a thin section of the ODS steel powder particle and perform the ACOM-TEM study. Relevant temperatures regarding recovery and recrystallization during the heat treatment had first been identified with XRD profile analysis. Selected states were further characterized using ACOM-TEM that provides key information on microstructure, i.e. grain size and morphology, crystallite size, local texture and distortion. ACOM-TEM cartographies have revealed for the first time that the microstructure of as-milled ODS ferritic steel particles consists in very anisotropic grains containing undistorted domains and dislocation walls. This is in agreement with the nanosized crystallites measured by XRD results. The mutual benefits of XRD and ACOM-TEM methods to analyse and describe the microstructure are discussed as well as the reliability of dislocation density measurements provided by ACOM-TEM misorientation measurements. In addition, of the ACOM-TEM results, the microstructural evolution during the processing route is interpreted in terms of a competition between recovery, recrystallization, grain growth and precipitation.