Mesoporous zeolite LTA-encapsulated Ni(II)-Schiff base complex: an efficient heterogeneous catalyst for electrocatalytic oxidation of methanol in alkaline media

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• 作者：Wenyang Wang ; Ruifeng Li ; Binbin Fan ; Jinghong Ma ; Rong Zhang
• 关键词：Encapsulation ; Methanol electrooxidation ; Schiff base complexes ; Nickel ; Mesoporous zeolite LTA
• 刊名：Ionics
• 出版年：2015
• 出版时间：September 2015
• 年：2015
• 卷：21
• 期：9
• 页码：2591-2602
• 全文大小：829 KB
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• 作者单位：Wenyang Wang (1) (2)
  Ruifeng Li (1) (2)
  Binbin Fan (2)
  Jinghong Ma (2)
  Rong Zhang (1)
  
  1. College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan, 030024, China
  2. Research Centre of Energy Chemical & Catalytic Technology, MOE, Institute of Special Chemicals, Taiyuan University of Technology, 79# West Yingze Street, Taiyuan, 030024, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Electrochemistry
  Materials Science
  Physical Chemistry
  Condensed Matter
  Renewable Energy Sources
  Electrical Power Generation and Transmission
  
• 出版者：Springer Berlin / Heidelberg
• ISSN：1862-0760

文摘

A series of Ni(II)-Schiff base complexes were encapsulated in mesoporous zeolite LTA (denoted as NiL/LTA with L-?salen, salpn, salbn, salphen, and tBu₄salen) and showed superior electrocatalytic activities for methanol oxidation in alkaline media. Different performances for methanol oxidation were due to the existence of different type of ligand that may originate from different steric and electronic effects exerted by the substituents present on the backbone of the salen ligands and/or by the different lengths of diamine bridge. The use of mesoporous zeolite LTA with nano-cages of 3 nm makes possible the interaction between the partially coordinated Ni(salen) in adjacent or appropriate sites in a nano-cage through the zeolite lattice oxygen, leading to the formation of new electrochemically accessible active sites and a great improvement in the electrocatalytic activities. A possible mechanism was proposed that electrocatalytic oxidation of methanol on NiL/LTA/GCEs was done by reaction with Ni(III)LO(OH) and also direct electro-oxidation reaction. Keywords Encapsulation Methanol electrooxidation Schiff base complexes Nickel Mesoporous zeolite LTA