A lexicon for consistent description of material images for nuclear forensics

详细信息    查看全文

• 作者：Alison L. Tamasi ; Leigh J. Cash…
• 关键词：Image ; Morphology ; Nuclear forensics ; Scanning electron microscopy ; Terminology ; Texture
• 刊名：Journal of Radioanalytical and Nuclear Chemistry
• 出版年：2016
• 出版时间：March 2016
• 年：2016
• 卷：307
• 期：3
• 页码：1611-1619
• 全文大小：2,417 KB
• 参考文献：1.Mayer K, Wallenius M, Varga Z (2013) Nulcear forensic science: correlating measurable material parameters to the history of nuclear material. Chem Rev 113:884–900CrossRef
  2.Moody KJ, Hutcheon ID, Grant PM (2005) Nuclear forensic analysis. Taylor & Francis, New YorkCrossRef
  3.Grant PM, Moody KJ, Hutcheon ID, Phinney DL, Whipple RE, Haas JS, Alcaraz A, Andrews JE, Klunder GL, Russo RE, Fickies TE, Pelkey GE, Andresen BD, Kruchten DA, Cantlin S (1998) Nuclear forensics in law enforcement applications. J Radioanal Nucl Chem 235:129–132CrossRef
  4.Shaban SE, Ibrahiem NM, El-mongy SA, Elshereafy EE (2013) Validation of scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and gamma spectrometry to verify source nuclear material for safeguards purposes. J Radioanal Nucl Chem 296:1219–1224CrossRef
  5.Martinez T, Lartigue J, Avila-Perez P, Carapio-Morales L, Zarazua G, Navarrete M, Tejeda S, Cabrera L (2008) Characterization of particulate matter from the Metropolitan Zone of the Valley of Mexico by scanning electron microscopy and energy dispersive X-ray analysis. J Radioanal Nucl Chem 276:799–806CrossRef
  6.Bowen J, Glover S, Spitz H (2013) Morphology of actinide-rich particles released from the BOMARC accident and collected from soil post remediation. J Radioanal Nucl Chem 296:853–857CrossRef
  7.Tsai T-L, Lin T-Y, Su T-Y, Wen T-J, Men L-C, Lin C-C (2013) Chemical and radiochemical analysis of corrosion products on BWR fuel surfaces. J Radioanal Nucl Chem 295:289–296CrossRef
  8.Paik S, Biswas S, Bhattacharya S, Roy SB (2013) Effect of ammonium nitrate on precipitation of ammonium di-uranate (ADU) and its characteristics. J Nucl Mater 440:34–38CrossRef
  9.Manna S, Karthik P, Mukherjee A, Banerjee J, Roy SB, Joshi JB (2012) Study of calcinations of ammonium diuranate at different temperatures. J Nucl Mater 426:229–232CrossRef
  10.Manna S, Roy SB, Joshi JB (2012) Study of crystallization and morphology ammonium diuranate and uranium oxide. J Nucl Mater 424:94–100CrossRef
  11.Kim K-W, Hyun J-T, Lee K-Y, Lee E-H, Lee K-W, Song K-C, Moon J-K (2011) Effects of the different conditions of uranyl and hydrogen peroxide solutions on the behavior of the uranium peroxide precipitation. J Hazard Mater 193:52–58CrossRef
  12.Krupka KM, Parkhurst MA, Gold K, Arey BW, Jenson ED, Guilmette RA (2009) Physicochemical characterization of capstone depleted uranium aerosols III: morphologic and chemical oxide analyses. Health Phys 96:276–291CrossRef
  13.Andreev EI, Glavin KB, Ivanov AV, Maloyik VV, Martynov VV, Panov VS (2009) Some results uranium dioxide powder structure investigation. Russ J Non-Ferr Met 50:281–285CrossRef
  14.Hastings EP, Lewis C, FitzPatrick J, Rademacher D, Tandon L (2008) Characterization of depleted uranium oxides fabricated using different processing methods. J Radioanal Nucl Chem 276:475–481CrossRef
  15.Marajofsky A, Perez L, Celora J (1991) On the dependence of characteristics of powders on the AUC process parameters. J Nucl Mater 178:143–151CrossRef
  16.Pan Y-M, Ma C-B, Hsu N-N (1981) The conversion of UO2 via ammonium uranyl carbonate: study of precipitation, chemical variation and powder properties. J Nucl Mater 99:135–147CrossRef
  17.Woolfrey JL (1978) The preparation of UO2 powder: effect of ammonium uranate properties. J Nucl Mater 74:123–131CrossRef
  18.Janov J, Alfredson PG, Vilkaitis VK (1972) The influence of precipitation conditions on the properties of ammonium diuranate and uranium dioxide powders. J Nucl Mater 44:161–174CrossRef
  19.Cordfunde EHP, van der Giessen AA (1967) Particle properties and sintering behavior of uranium dioxide. J Nucl Mater 24:141–149CrossRef
  20.Doi H, Ito T (1964) Significance of physical state of starting precipitate in growth of uranium dioxide particles. J Nucl Mater 11:94–106CrossRef
  21.Miller NA, Henderson JJ (2010) Quantifying sand particle shape complexity using a dynamic, digital imaging technique. Agron J 102:1407–1414CrossRef
  22.Walton DE, Mumford CJ (1999) Spray dried products—characterization of particle morphology. Chem Eng Res Des 77:21–38CrossRef
  23. http://​www.​mama.​lanl.​gov
  
• 作者单位：Alison L. Tamasi (1) (2)
  Leigh J. Cash (1)
  Christopher Eley (3)
  Reid B. Porter (1)
  David L. Pugmire (1)
  Amy R. Ross (1)
  Christy E. Ruggiero (1)
  Lav Tandon (1)
  Gregory L. Wagner (1)
  Justin R. Walensky (2)
  Angelique D. Wall (1)
  Marianne P. Wilkerson (1)
  
  1. Los Alamos National Laboratory, P.O. Box 1663, Los Alamos, NM, 87545, USA
  2. Department of Chemistry, University of Missouri-Columbia, Columbia, MO, 65211, USA
  3. Department of Chemistry, South Carolina State University, Orangeburg, SC, 29117, USA
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Nuclear Chemistry
  Physical Chemistry
  Nuclear Physics, Heavy Ions and Hadrons
  Diagnostic Radiology
  Inorganic Chemistry
  
• 出版者：Akad茅miai Kiad贸, co-published with Springer Science+Business Media B.V., Formerly Kluwer Academic
• ISSN：1588-2780

文摘

We have developed a lexicon to consistently and objectively describe morphological features observed in scanning electron microscopy (SEM) images. Here we provide the lexicon flowsheet, define the terminology, and detail step-by-step characterization of SEM images collected from a set of actinide oxides. We conclude that this lexicon can be used to characterize texture and surface features, particle structure and size, and grain boundaries in an image of a material. The lexicon should be applicable to characterization of images collected from other techniques for measuring morphology, as well. LA-UR-15-26746