生活饮用水中半挥发性有机污染物残留检测
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摘要
介绍了生活饮用水中半挥发性有机污染物的前处理和检测方法,综述了液液萃取、固相萃取、固相微萃取、液液微萃取、中空纤维膜萃取和固相膜萃取等样品预处理方法以及对半挥发性有机物检测分析的相关方法,并对生活饮用水中的半挥发性有机污染物的检测研究进行了展望,旨在为水中半挥发性有机物检测提供一定参考。
This paper introduces the pre processing and detection method of semi volatile organic pollutants in drinking water, the paper summarized the methods of liquid-liquid extraction, solid-phase extraction, solid-phase microextraction,liquid phase micro extraction, hollow fiber membrane extraction and solid phase extraction, sample pretreatment, and on the analysis of the essential correlation detection method of organic matter, and progress on determination of semi volatile organic pollutants in drinking water are discussed. The purpose is to provide a reference for the detection of semi volatile organic compounds in water.
This paper introduces the pre processing and detection method of semi volatile organic pollutants in drinking water, the paper summarized the methods of liquid-liquid extraction, solid-phase extraction, solid-phase microextraction,liquid phase micro extraction, hollow fiber membrane extraction and solid phase extraction, sample pretreatment, and on the analysis of the essential correlation detection method of organic matter, and progress on determination of semi volatile organic pollutants in drinking water are discussed. The purpose is to provide a reference for the detection of semi volatile organic compounds in water.
引文
[1] MADER B T,PANKOW J F. Gas/solid panritioning of semiwolatile organic compounds(SOCs)to air filter.3.An analysis of gas adsorption artifacts in measurements of atmospheric SOCs and organic carbon(OC)when using Teflon membrane filters and quartz fiber filters[J].Eneiron Sci Technol,2011,35(17):3422-3432.
[2]高缨红.水中半挥发性有机物分析方法研究进展[J].广州化工,2013,40(18):75-76.
[3]孔德洋,何健,许静,等.串联固相萃取-气相色谱法同时测定水体中25种有机氯农药痕量残留[J].环境化学,2013(12):2398-2399.
[4]邹琴,刘守亮,秦启发,等.环境与食品中有机氯农药残留及降解的调查分析[J].公共卫生与预防医学,2010,21(1):37-39.
[5] GB 5749-2006,生活饮用水卫生标准[S].
[6]中华人民共和国卫生部.生活饮用水标准检验方法:GB/T 5750.8-2006[S].北京:中国标准出版社,2006:101-115.
[7]李垚辛,董全.有机磷农药残留检测技术的研究进展[J].中国食品与营养,2010(4):12-15.
[8]梁素丹,陈剑刚,白艳玲,等.液液萃取-气相色谱法同时测定水中氯苯类化合物和有机氯农药[J].中国卫生检验杂志,2013,23(6):1385-1388.
[9]杨冉,刘菲.不同p H调节顺序对水中半挥发性有机物提取效率的研究[J].分析实验室,2013,32(2):77-79.
[10] LIU H J,DASGUPTA P K. Analytical chemistry in a drop solvent extraction in a microdrop[J].Trends Anal Chem,1996,68(11):1817-1821.
[11]刁春鹏,时军波,苑金鹏,等.中空纤维液相微萃取技术及其应用进展[J].光谱实验室,2008,25(2):158-163.
[12] REZAEE M,ASSADI Y,HOSSEINI M R M,et al. Determination of organic compounds in water using dispersive liquidliquid microextraction[J].Chromatogr A,2006,1116:1-9.
[13]陈波,靳保辉,肖锋,等.分散液液微萃取-保留时间锁定-气相色谱质谱联用测定地表水中34种农药[J].中国卫生检验杂志,2013,23(16):3181-3189.
[14] ZANJANI M R K,YAMINI Y,SHARIATI S,et al. Applications of liquid-phase microextraction techniques in natural product analysis[J].Anal Chimacta,2007,585(2):286-289.
[15]李晓霞,王宇,雍莉,等.悬浮固化液相微萃取-气相色谱法测定水中有机氯农药[J].四川大学学报(医学版),2014,45(2):324-327.
[16] LEONG M I,HUANG S D.Dispersive liquid-liquid microextraction method based on solidification of floating organic drop combined with gas chromatography with electron-capture or mass spectrometry detection[J].J Chromatogr A,2008,1211(1-2):8-12.
[17] ZACHARIS C K,TZANAVARAS P D, ROUBOS K,et al. Reviews in pharmaceutical and biomedical analysis?[J].Chromatogr A,2010,1217:5896-5899.
[18]王宇,朱成华,邹晓莉,等.溶剂去乳化-悬浮固化分散液液微萃取-气相色谱-质谱联用测定水中的有机氯农药[J].色谱,2013,31(11):1076-1080.
[19]李刚,张占恩.中空纤维膜液相微萃取-气相色谱-质谱法测定水样中拟除虫菊酯类农药[J].理化检验-化学分册,2010,46(3):227-229.
[20]张文文,孟品佳,孟梁,等.中空纤维膜液相萃取-气相色谱-质谱法测定尿液中的苯丙胺类兴奋剂[J].分析实验室,2013,32(1):44-47.
[21]储险峰,徐洁,康长安,等.中空纤维膜萃取-气相色谱法测定水中有机氯农药[J].中国环境监测,2014,30(3):140-143.
[22]汪雨,支辛辛,张玲金,等.利用碳纳米管固相萃取气相色谱法对水中有机氯农药和多氯联苯的测定[J].分析测试学报,2008,27(5):493-496.
[23]王鑫,许小苗,愈晔,等.固相萃取-气相色谱法测定水中酞酸酯类环境激素[J].食品工业科技,2008,29(4):287-289.
[24]郑能雄,林华影,柯华,等.固相萃取/气相色谱-质谱联用法同时测定水中116种半挥发性有机物[J].中国卫生检验杂志,2010,20(7):1593-1596.
[25]李凌,张付刚,李健,等.固相萃取-气质联用测定水中23种有机氯有机磷农药污染物[J].环境卫生学杂志,2014,4(3):305-309.
[26]陈军,张宗祥,杨文武,等.固相萃取-气质联用法测定水中有机氯农药和氯苯类化合物[J].环境监测管理与技术,2015,27(1):46-49.
[27]任琳,秦忠雪,朱婧,等.固相萃取-气相色谱-串联质谱法测定水中16种有机磷和有机氯农药残留[J].中国卫生检验杂志,2017,27(10):1396-1399.
[28]肖红,王巧丽,王朝阳,等.全自动C-18膜固相萃取-气相色谱法测定水中有机氯农药[J].化学工程师,2016,30(9):30-33.
[29]许百环.固相萃取-高效液相色谱法同时测定水中甲萘威、阿特拉津和苯并[a]芘[J].福建分析测试,2017,28(2):14-18.
[30]王敏,李广益,高慧,等.高效液相色谱法-柱后衍生测定水中草甘膦[J].食品科技,2017,12(2):39-42.
[31]梁素丹,陈剑刚,白艳玲,等.液液萃取-气相色谱法同时测定水中氯苯类化合物和有机氯农药[J].中国卫生检验杂志,2013,23(6):1385-1388.
[32]吴春英,谷风,白鹭,等.固相萃取-超高效液相色谱-三重四极杆质谱联用同时测定水中菊酯类农药多残留[J].分析科学学报,2017,33(1):57-62.
[2]高缨红.水中半挥发性有机物分析方法研究进展[J].广州化工,2013,40(18):75-76.
[3]孔德洋,何健,许静,等.串联固相萃取-气相色谱法同时测定水体中25种有机氯农药痕量残留[J].环境化学,2013(12):2398-2399.
[4]邹琴,刘守亮,秦启发,等.环境与食品中有机氯农药残留及降解的调查分析[J].公共卫生与预防医学,2010,21(1):37-39.
[5] GB 5749-2006,生活饮用水卫生标准[S].
[6]中华人民共和国卫生部.生活饮用水标准检验方法:GB/T 5750.8-2006[S].北京:中国标准出版社,2006:101-115.
[7]李垚辛,董全.有机磷农药残留检测技术的研究进展[J].中国食品与营养,2010(4):12-15.
[8]梁素丹,陈剑刚,白艳玲,等.液液萃取-气相色谱法同时测定水中氯苯类化合物和有机氯农药[J].中国卫生检验杂志,2013,23(6):1385-1388.
[9]杨冉,刘菲.不同p H调节顺序对水中半挥发性有机物提取效率的研究[J].分析实验室,2013,32(2):77-79.
[10] LIU H J,DASGUPTA P K. Analytical chemistry in a drop solvent extraction in a microdrop[J].Trends Anal Chem,1996,68(11):1817-1821.
[11]刁春鹏,时军波,苑金鹏,等.中空纤维液相微萃取技术及其应用进展[J].光谱实验室,2008,25(2):158-163.
[12] REZAEE M,ASSADI Y,HOSSEINI M R M,et al. Determination of organic compounds in water using dispersive liquidliquid microextraction[J].Chromatogr A,2006,1116:1-9.
[13]陈波,靳保辉,肖锋,等.分散液液微萃取-保留时间锁定-气相色谱质谱联用测定地表水中34种农药[J].中国卫生检验杂志,2013,23(16):3181-3189.
[14] ZANJANI M R K,YAMINI Y,SHARIATI S,et al. Applications of liquid-phase microextraction techniques in natural product analysis[J].Anal Chimacta,2007,585(2):286-289.
[15]李晓霞,王宇,雍莉,等.悬浮固化液相微萃取-气相色谱法测定水中有机氯农药[J].四川大学学报(医学版),2014,45(2):324-327.
[16] LEONG M I,HUANG S D.Dispersive liquid-liquid microextraction method based on solidification of floating organic drop combined with gas chromatography with electron-capture or mass spectrometry detection[J].J Chromatogr A,2008,1211(1-2):8-12.
[17] ZACHARIS C K,TZANAVARAS P D, ROUBOS K,et al. Reviews in pharmaceutical and biomedical analysis?[J].Chromatogr A,2010,1217:5896-5899.
[18]王宇,朱成华,邹晓莉,等.溶剂去乳化-悬浮固化分散液液微萃取-气相色谱-质谱联用测定水中的有机氯农药[J].色谱,2013,31(11):1076-1080.
[19]李刚,张占恩.中空纤维膜液相微萃取-气相色谱-质谱法测定水样中拟除虫菊酯类农药[J].理化检验-化学分册,2010,46(3):227-229.
[20]张文文,孟品佳,孟梁,等.中空纤维膜液相萃取-气相色谱-质谱法测定尿液中的苯丙胺类兴奋剂[J].分析实验室,2013,32(1):44-47.
[21]储险峰,徐洁,康长安,等.中空纤维膜萃取-气相色谱法测定水中有机氯农药[J].中国环境监测,2014,30(3):140-143.
[22]汪雨,支辛辛,张玲金,等.利用碳纳米管固相萃取气相色谱法对水中有机氯农药和多氯联苯的测定[J].分析测试学报,2008,27(5):493-496.
[23]王鑫,许小苗,愈晔,等.固相萃取-气相色谱法测定水中酞酸酯类环境激素[J].食品工业科技,2008,29(4):287-289.
[24]郑能雄,林华影,柯华,等.固相萃取/气相色谱-质谱联用法同时测定水中116种半挥发性有机物[J].中国卫生检验杂志,2010,20(7):1593-1596.
[25]李凌,张付刚,李健,等.固相萃取-气质联用测定水中23种有机氯有机磷农药污染物[J].环境卫生学杂志,2014,4(3):305-309.
[26]陈军,张宗祥,杨文武,等.固相萃取-气质联用法测定水中有机氯农药和氯苯类化合物[J].环境监测管理与技术,2015,27(1):46-49.
[27]任琳,秦忠雪,朱婧,等.固相萃取-气相色谱-串联质谱法测定水中16种有机磷和有机氯农药残留[J].中国卫生检验杂志,2017,27(10):1396-1399.
[28]肖红,王巧丽,王朝阳,等.全自动C-18膜固相萃取-气相色谱法测定水中有机氯农药[J].化学工程师,2016,30(9):30-33.
[29]许百环.固相萃取-高效液相色谱法同时测定水中甲萘威、阿特拉津和苯并[a]芘[J].福建分析测试,2017,28(2):14-18.
[30]王敏,李广益,高慧,等.高效液相色谱法-柱后衍生测定水中草甘膦[J].食品科技,2017,12(2):39-42.
[31]梁素丹,陈剑刚,白艳玲,等.液液萃取-气相色谱法同时测定水中氯苯类化合物和有机氯农药[J].中国卫生检验杂志,2013,23(6):1385-1388.
[32]吴春英,谷风,白鹭,等.固相萃取-超高效液相色谱-三重四极杆质谱联用同时测定水中菊酯类农药多残留[J].分析科学学报,2017,33(1):57-62.
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